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Main Authors: Butcher, T. A., Prendeville, L., Rafferty, A., Trtik, P., Boillat, P., Coey, J. M. D.
Format: Preprint
Published: 2021
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Online Access:https://arxiv.org/abs/2107.02770
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author Butcher, T. A.
Prendeville, L.
Rafferty, A.
Trtik, P.
Boillat, P.
Coey, J. M. D.
author_facet Butcher, T. A.
Prendeville, L.
Rafferty, A.
Trtik, P.
Boillat, P.
Coey, J. M. D.
contents The electrosorption of Gd$^{3+}$ ions from aqueous 70 mM Gd(NO$_3$)$_3$ solution in monolithic carbon aerogel electrodes was recorded by dynamic neutron imaging. The aerogels have a bimodal pore size distribution consisting of macropores and mesopores centered at 115 nm and 15 nm, respectively. After the uptake of Gd$^{3+}$ ions by the negatively charged surface of the porous structure, an inhomogeneous magnetic field was applied to the system of discharging electrodes. This led to a convective flow and confinement of Gd(NO$_3$)$_3$ solution in the magnetic field gradient. Thus, a way to desalt and capture paramagnetic ions from an initially homogeneous solution is established.
format Preprint
id arxiv_https___arxiv_org_abs_2107_02770
institution arXiv
publishDate 2021
record_format arxiv
spellingShingle Neutron Imaging of Paramagnetic Ions: Electrosorption by Carbon Aerogels and Macroscopic Magnetic Forces
Butcher, T. A.
Prendeville, L.
Rafferty, A.
Trtik, P.
Boillat, P.
Coey, J. M. D.
Chemical Physics
The electrosorption of Gd$^{3+}$ ions from aqueous 70 mM Gd(NO$_3$)$_3$ solution in monolithic carbon aerogel electrodes was recorded by dynamic neutron imaging. The aerogels have a bimodal pore size distribution consisting of macropores and mesopores centered at 115 nm and 15 nm, respectively. After the uptake of Gd$^{3+}$ ions by the negatively charged surface of the porous structure, an inhomogeneous magnetic field was applied to the system of discharging electrodes. This led to a convective flow and confinement of Gd(NO$_3$)$_3$ solution in the magnetic field gradient. Thus, a way to desalt and capture paramagnetic ions from an initially homogeneous solution is established.
title Neutron Imaging of Paramagnetic Ions: Electrosorption by Carbon Aerogels and Macroscopic Magnetic Forces
topic Chemical Physics
url https://arxiv.org/abs/2107.02770