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| Main Authors: | , |
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| Format: | Preprint |
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2023
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| Online Access: | https://arxiv.org/abs/2310.10786 |
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| _version_ | 1866917754948288512 |
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| author | Moradi, Hamidreza Mehradnia, Fatemeh |
| author_facet | Moradi, Hamidreza Mehradnia, Fatemeh |
| contents | The X-ray diffractometer in the laboratory is a crucial instrument for analyzing materials in science. It can be used on almost any crystal material, and if the machine parameters are appropriately controlled, it can offer a lot of information about the samples characteristics. Nevertheless, the data obtained from these machines are complicated by an aberration function that can be resolved through calibration. In this study, a powder comprising of Barium Sulfate (BaSO4), Zinc Oxide (ZnO) and Aluminum (Al) was used as the first sample and a single crystal sample comprised of Gallium Nitride (GaN) and Aluminum Oxide (Al2O3). The required calibration parameters of the X-ray diffractometer namely: Straight Beam Alignment, Beam Cut Alignment and Sample Tilt Alignment for two samples were analyzed and carried out. Using the results of the X-ray spectrum, important parameters such as corresponding planes for peak positions, d-spacing of planes, intensities, smallest crystallite sizes and lattice parameters, and a comparison with the reference data were all carried out. As another result, the out-of-plane alignment and Full-Width at Half-Maximum (FWHM) value for GaN could be determined using the rocking curve. |
| format | Preprint |
| id |
arxiv_https___arxiv_org_abs_2310_10786 |
| institution | arXiv |
| publishDate | 2023 |
| record_format | arxiv |
| spellingShingle | An analysis on improvement of x-ray diffractometer results by controlling and calibration of parameters Moradi, Hamidreza Mehradnia, Fatemeh Applied Physics The X-ray diffractometer in the laboratory is a crucial instrument for analyzing materials in science. It can be used on almost any crystal material, and if the machine parameters are appropriately controlled, it can offer a lot of information about the samples characteristics. Nevertheless, the data obtained from these machines are complicated by an aberration function that can be resolved through calibration. In this study, a powder comprising of Barium Sulfate (BaSO4), Zinc Oxide (ZnO) and Aluminum (Al) was used as the first sample and a single crystal sample comprised of Gallium Nitride (GaN) and Aluminum Oxide (Al2O3). The required calibration parameters of the X-ray diffractometer namely: Straight Beam Alignment, Beam Cut Alignment and Sample Tilt Alignment for two samples were analyzed and carried out. Using the results of the X-ray spectrum, important parameters such as corresponding planes for peak positions, d-spacing of planes, intensities, smallest crystallite sizes and lattice parameters, and a comparison with the reference data were all carried out. As another result, the out-of-plane alignment and Full-Width at Half-Maximum (FWHM) value for GaN could be determined using the rocking curve. |
| title | An analysis on improvement of x-ray diffractometer results by controlling and calibration of parameters |
| topic | Applied Physics |
| url | https://arxiv.org/abs/2310.10786 |