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Main Authors: Åsland, Anna Cecilie, Cooil, Simon P., Mamedov, Damir, Røst, Håkon I., Bakkelund, Johannes, Li, Zheshen, Karazhanov, Smagul, Wells, Justin W.
Format: Preprint
Published: 2023
Subjects:
Online Access:https://arxiv.org/abs/2311.04639
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author Åsland, Anna Cecilie
Cooil, Simon P.
Mamedov, Damir
Røst, Håkon I.
Bakkelund, Johannes
Li, Zheshen
Karazhanov, Smagul
Wells, Justin W.
author_facet Åsland, Anna Cecilie
Cooil, Simon P.
Mamedov, Damir
Røst, Håkon I.
Bakkelund, Johannes
Li, Zheshen
Karazhanov, Smagul
Wells, Justin W.
contents Anti-icing coatings are intended to prevent ice formation on surfaces, minimising the risk of surface-related damage and also reducing ice-related hazards in society. $\mathrm{CeO}_{2}$ coatings are robust, hydrophobic, and transmit light, thus they are suitable for a range of applications. However, their evolving surface chemistry during the initial stages of $\mathrm{H}_{2}\mathrm{O}$ exposure at very low temperatures has not been investigated, despite that this is important for understanding their anti-icing properties. To study this, $\mathrm{CeO}_{2}$ coatings were grown by sputter deposition, cooled to $\approx100\,$K and exposed to a $\mathrm{H}_{2}\mathrm{O}$ atmosphere at $1\times10^{-8}\,\mathrm{mbar}$. We demonstrate the usefulness of X-ray photoelectron spectroscopy (XPS) as a tool for investigating the anti-icing properties of surfaces. We present XPS measurements of $\mathrm{CeO}_{2}$ coatings before and after exposure to $\mathrm{H}_{2}\mathrm{O}$, in-situ and at cryogenic temperatures. XPS reveals that little to no ice forms on the surface of $\mathrm{CeO}_{2}$ after the $\mathrm{H}_{2}\mathrm{O}$ exposure at $\approx100\,$K. In contrast, ice was observed all over the sample holder on which the $\mathrm{CeO}_{2}$ was mounted. These findings suggest that $\mathrm{CeO}_{2}$ is a promising candidate for future anti-icing coatings.
format Preprint
id arxiv_https___arxiv_org_abs_2311_04639
institution arXiv
publishDate 2023
record_format arxiv
spellingShingle Initial Stages of Water Absorption on $\mathbf{CeO}_{2}$ Surfaces at Very Low Temperatures for Understanding Anti-Icing Coatings
Åsland, Anna Cecilie
Cooil, Simon P.
Mamedov, Damir
Røst, Håkon I.
Bakkelund, Johannes
Li, Zheshen
Karazhanov, Smagul
Wells, Justin W.
Chemical Physics
Anti-icing coatings are intended to prevent ice formation on surfaces, minimising the risk of surface-related damage and also reducing ice-related hazards in society. $\mathrm{CeO}_{2}$ coatings are robust, hydrophobic, and transmit light, thus they are suitable for a range of applications. However, their evolving surface chemistry during the initial stages of $\mathrm{H}_{2}\mathrm{O}$ exposure at very low temperatures has not been investigated, despite that this is important for understanding their anti-icing properties. To study this, $\mathrm{CeO}_{2}$ coatings were grown by sputter deposition, cooled to $\approx100\,$K and exposed to a $\mathrm{H}_{2}\mathrm{O}$ atmosphere at $1\times10^{-8}\,\mathrm{mbar}$. We demonstrate the usefulness of X-ray photoelectron spectroscopy (XPS) as a tool for investigating the anti-icing properties of surfaces. We present XPS measurements of $\mathrm{CeO}_{2}$ coatings before and after exposure to $\mathrm{H}_{2}\mathrm{O}$, in-situ and at cryogenic temperatures. XPS reveals that little to no ice forms on the surface of $\mathrm{CeO}_{2}$ after the $\mathrm{H}_{2}\mathrm{O}$ exposure at $\approx100\,$K. In contrast, ice was observed all over the sample holder on which the $\mathrm{CeO}_{2}$ was mounted. These findings suggest that $\mathrm{CeO}_{2}$ is a promising candidate for future anti-icing coatings.
title Initial Stages of Water Absorption on $\mathbf{CeO}_{2}$ Surfaces at Very Low Temperatures for Understanding Anti-Icing Coatings
topic Chemical Physics
url https://arxiv.org/abs/2311.04639