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Autori principali: Gao, Ran, Jin, Lun, Huyan, Shuyuan, Ni, Danrui, Wang, Haozhe, Xu, Xianghan, Budko, Sergey L., Canfield, Paul, Xie, Weiwei, Cava, Robert J.
Natura: Preprint
Pubblicazione: 2023
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Accesso online:https://arxiv.org/abs/2311.11122
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author Gao, Ran
Jin, Lun
Huyan, Shuyuan
Ni, Danrui
Wang, Haozhe
Xu, Xianghan
Budko, Sergey L.
Canfield, Paul
Xie, Weiwei
Cava, Robert J.
author_facet Gao, Ran
Jin, Lun
Huyan, Shuyuan
Ni, Danrui
Wang, Haozhe
Xu, Xianghan
Budko, Sergey L.
Canfield, Paul
Xie, Weiwei
Cava, Robert J.
contents Superconducting states onsetting at moderately high temperatures have been observed in epitaxially-stabilized RENiO2-based thin films. However, recently it has also been reported that superconductivity at high temperatures is observed in bulk La3Ni2O7-δ at high pressure, opening further possibilities for study. Here we report the reduction profile of La3Ni2O7 in a stream of 5% H2/Ar gas and the isolation of the metastable intermediate phase La3Ni2O6.45, which is based on Ni2+. Although this reduced phase does not superconduct at ambient or high pressures, it offers insights into the Ni-327 system and encourages the future study of nickelates as a function of oxygen content.
format Preprint
id arxiv_https___arxiv_org_abs_2311_11122
institution arXiv
publishDate 2023
record_format arxiv
spellingShingle Is La3Ni2O6.5 a Bulk Superconducting Nickelate?
Gao, Ran
Jin, Lun
Huyan, Shuyuan
Ni, Danrui
Wang, Haozhe
Xu, Xianghan
Budko, Sergey L.
Canfield, Paul
Xie, Weiwei
Cava, Robert J.
Materials Science
Superconducting states onsetting at moderately high temperatures have been observed in epitaxially-stabilized RENiO2-based thin films. However, recently it has also been reported that superconductivity at high temperatures is observed in bulk La3Ni2O7-δ at high pressure, opening further possibilities for study. Here we report the reduction profile of La3Ni2O7 in a stream of 5% H2/Ar gas and the isolation of the metastable intermediate phase La3Ni2O6.45, which is based on Ni2+. Although this reduced phase does not superconduct at ambient or high pressures, it offers insights into the Ni-327 system and encourages the future study of nickelates as a function of oxygen content.
title Is La3Ni2O6.5 a Bulk Superconducting Nickelate?
topic Materials Science
url https://arxiv.org/abs/2311.11122