Demonstration and STEM Analysis of Ferroelectric Switching in MOCVD-Grown Single Crystalline Al$_{0.85}$Sc$_{0.15}$N

Fuente: arXiv
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Main Authors: Wolff, Niklas, Schoenweger, Georg, Streicher, Isabel, Islam, Md Redwanul, Braun, Nils, Stranak, Patrik, Kirste, Lutz, Prescher, Mario, Lotnyk, Andriy, Kohlstedt, Hermann, Leone, Stefano, Kienle, Lorenz, Fichtner, Simon
Format: Preprint
Published: 2023
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author Wolff, Niklas
Schoenweger, Georg
Streicher, Isabel
Islam, Md Redwanul
Braun, Nils
Stranak, Patrik
Kirste, Lutz
Prescher, Mario
Lotnyk, Andriy
Kohlstedt, Hermann
Leone, Stefano
Kienle, Lorenz
Fichtner, Simon
author_facet Wolff, Niklas
Schoenweger, Georg
Streicher, Isabel
Islam, Md Redwanul
Braun, Nils
Stranak, Patrik
Kirste, Lutz
Prescher, Mario
Lotnyk, Andriy
Kohlstedt, Hermann
Leone, Stefano
Kienle, Lorenz
Fichtner, Simon
contents Wurtzite-type Al$_{1-x}$Sc$_x$N solid solutions grown by metal organic chemical vapour deposition are for the first time confirmed to be ferroelectric. The film with 230 nm thickness and x = 0.15 exhibits a coercive field of 5.5 MV/cm at a measurement frequency of 1.5 kHz. Single crystal quality and homogeneous chemical composition of the film was confirmed by X-ray diffraction spectroscopic methods such as time of flight secondary ion mass spectrometry. Annular bright field scanning transmission electron microscopy served to proof the ferroelectric polarization inversion on unit cell level. The single crystal quality further allowed to image the large-scale domain pattern of a wurtzite-type ferroelectric for the first time, revealing a predominantly cone-like domain shape along the c-axis of the material. As in previous work, this again implies the presence of strong polarization discontinuities along this crystallographic axis, which could be suitable for current transport. The domains are separated by narrow domain walls, for which an upper thickness limit of 3 nm was deduced, but which could potentially be atomically sharp. We are confident that these results will advance the commencing integration of wurtzite-type ferroelectrics to GaN as well as generally III-N based heterostructures and devices.
format Preprint
id arxiv_https___arxiv_org_abs_2312_13759
institution arXiv
publishDate 2023
record_format arxiv
spellingShingle Demonstration and STEM Analysis of Ferroelectric Switching in MOCVD-Grown Single Crystalline Al$_{0.85}$Sc$_{0.15}$N
Wolff, Niklas
Schoenweger, Georg
Streicher, Isabel
Islam, Md Redwanul
Braun, Nils
Stranak, Patrik
Kirste, Lutz
Prescher, Mario
Lotnyk, Andriy
Kohlstedt, Hermann
Leone, Stefano
Kienle, Lorenz
Fichtner, Simon
Applied Physics
Materials Science
Wurtzite-type Al$_{1-x}$Sc$_x$N solid solutions grown by metal organic chemical vapour deposition are for the first time confirmed to be ferroelectric. The film with 230 nm thickness and x = 0.15 exhibits a coercive field of 5.5 MV/cm at a measurement frequency of 1.5 kHz. Single crystal quality and homogeneous chemical composition of the film was confirmed by X-ray diffraction spectroscopic methods such as time of flight secondary ion mass spectrometry. Annular bright field scanning transmission electron microscopy served to proof the ferroelectric polarization inversion on unit cell level. The single crystal quality further allowed to image the large-scale domain pattern of a wurtzite-type ferroelectric for the first time, revealing a predominantly cone-like domain shape along the c-axis of the material. As in previous work, this again implies the presence of strong polarization discontinuities along this crystallographic axis, which could be suitable for current transport. The domains are separated by narrow domain walls, for which an upper thickness limit of 3 nm was deduced, but which could potentially be atomically sharp. We are confident that these results will advance the commencing integration of wurtzite-type ferroelectrics to GaN as well as generally III-N based heterostructures and devices.
title Demonstration and STEM Analysis of Ferroelectric Switching in MOCVD-Grown Single Crystalline Al$_{0.85}$Sc$_{0.15}$N
topic Applied Physics
Materials Science
url https://arxiv.org/abs/2312.13759