Ultra-Cold Cryogenic TEM with Liquid Helium and High Stability

Fuente: arXiv
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Auteurs principaux: Rennich, Emily, Sung, Suk Hyun, Agarwal, Nishkarsh, Gates, Maya, Kerns, Robert, Hovden, Robert, Baggari, Ismail El
Format: Preprint
Publié: 2024
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author Rennich, Emily
Sung, Suk Hyun
Agarwal, Nishkarsh
Gates, Maya
Kerns, Robert
Hovden, Robert
Baggari, Ismail El
author_facet Rennich, Emily
Sung, Suk Hyun
Agarwal, Nishkarsh
Gates, Maya
Kerns, Robert
Hovden, Robert
Baggari, Ismail El
contents Cryogenic transmission electron microscopy has revolutionized structural biology and materials science, but achieving temperatures below the boiling point of liquid nitrogen remains a long-standing aspiration. We introduce an ultra-cold liquid helium transmission electron microscope specimen holder, featuring continuous cryogen flow and vibration decoupling. This instrument is compatible with modern aberration-corrected microscopes and achieves sub-25 K base temperature, ${\pm}$2 mK thermal stability over many hours, and atomic resolution--setting the stage for a new era of cryogenic electron microscopy.
format Preprint
id arxiv_https___arxiv_org_abs_2402_00636
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Ultra-Cold Cryogenic TEM with Liquid Helium and High Stability
Rennich, Emily
Sung, Suk Hyun
Agarwal, Nishkarsh
Gates, Maya
Kerns, Robert
Hovden, Robert
Baggari, Ismail El
Applied Physics
Cryogenic transmission electron microscopy has revolutionized structural biology and materials science, but achieving temperatures below the boiling point of liquid nitrogen remains a long-standing aspiration. We introduce an ultra-cold liquid helium transmission electron microscope specimen holder, featuring continuous cryogen flow and vibration decoupling. This instrument is compatible with modern aberration-corrected microscopes and achieves sub-25 K base temperature, ${\pm}$2 mK thermal stability over many hours, and atomic resolution--setting the stage for a new era of cryogenic electron microscopy.
title Ultra-Cold Cryogenic TEM with Liquid Helium and High Stability
topic Applied Physics
url https://arxiv.org/abs/2402.00636