Automated Tabletop Exfoliation and Identification of Monolayer Graphene Flakes

Fuente: arXiv
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Main Authors: Courtney, Elijah D. S., Pendharkar, Mihir, Bittner, Nathan J., Sharpe, Aaron L., Goldhaber-Gordon, David
Format: Preprint
Published: 2024
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author Courtney, Elijah D. S.
Pendharkar, Mihir
Bittner, Nathan J.
Sharpe, Aaron L.
Goldhaber-Gordon, David
author_facet Courtney, Elijah D. S.
Pendharkar, Mihir
Bittner, Nathan J.
Sharpe, Aaron L.
Goldhaber-Gordon, David
contents Over the past two decades, graphene has been intensively studied because of its remarkable mechanical, optical, and electronic properties. Initial studies were enabled by manual ``Scotch Tape'' exfoliation; nearly two decades later, this method is still widely used to obtain chemically-pristine flakes of graphene and other 2D van der Waals materials. Unfortunately, the yield of large, pristine flakes with uniform thickness is inconsistent. Thus, significant time and effort are required to exfoliate and locate flakes suitable for fabricating multilayer van der Waals heterostructures. Here, we describe a relatively affordable tabletop device (the ``eXfoliator'') that can reproducibly control key parameters and largely automate the exfoliation process. In a typical exfoliation run, the eXfoliator produces 3 or more large ($\ge400\ μ$m$^2$) high-quality graphene monolayer flakes, allowing new users to produce such flakes at a rate comparable to manual exfoliation by an experienced user. We use an automated mapping system and a computer vision algorithm to locate candidate flakes. Our results provide a starting point for future research efforts to more precisely identify which parameters matter for the success of exfoliation, and to optimize them.
format Preprint
id arxiv_https___arxiv_org_abs_2403_12901
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Automated Tabletop Exfoliation and Identification of Monolayer Graphene Flakes
Courtney, Elijah D. S.
Pendharkar, Mihir
Bittner, Nathan J.
Sharpe, Aaron L.
Goldhaber-Gordon, David
Mesoscale and Nanoscale Physics
Over the past two decades, graphene has been intensively studied because of its remarkable mechanical, optical, and electronic properties. Initial studies were enabled by manual ``Scotch Tape'' exfoliation; nearly two decades later, this method is still widely used to obtain chemically-pristine flakes of graphene and other 2D van der Waals materials. Unfortunately, the yield of large, pristine flakes with uniform thickness is inconsistent. Thus, significant time and effort are required to exfoliate and locate flakes suitable for fabricating multilayer van der Waals heterostructures. Here, we describe a relatively affordable tabletop device (the ``eXfoliator'') that can reproducibly control key parameters and largely automate the exfoliation process. In a typical exfoliation run, the eXfoliator produces 3 or more large ($\ge400\ μ$m$^2$) high-quality graphene monolayer flakes, allowing new users to produce such flakes at a rate comparable to manual exfoliation by an experienced user. We use an automated mapping system and a computer vision algorithm to locate candidate flakes. Our results provide a starting point for future research efforts to more precisely identify which parameters matter for the success of exfoliation, and to optimize them.
title Automated Tabletop Exfoliation and Identification of Monolayer Graphene Flakes
topic Mesoscale and Nanoscale Physics
url https://arxiv.org/abs/2403.12901