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Main Authors: Beechem, Thomas E, Vega, Fernando, Jaszewski, Samantha T., Aronson, Benjamin L., Kelley, Kyle P., Ihlefeld, Jon F.
Format: Preprint
Published: 2024
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Online Access:https://arxiv.org/abs/2406.11763
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author Beechem, Thomas E
Vega, Fernando
Jaszewski, Samantha T.
Aronson, Benjamin L.
Kelley, Kyle P.
Ihlefeld, Jon F.
author_facet Beechem, Thomas E
Vega, Fernando
Jaszewski, Samantha T.
Aronson, Benjamin L.
Kelley, Kyle P.
Ihlefeld, Jon F.
contents Photoinduced reductions in the oxygen vacancy concentration were leveraged to increase the ferroelectric phase fraction of $\mathrm{Hf_{0.5}Zr_{0.5}O_2}$ (HZO) thin-films. Modest ($\sim 0.02-0.77~\mathrm{mJ/μm^2}$) laser doses of visible light (488 nm, 2.54 eV) spatially patterned the concentration of oxygen vacancies as monitored by photoluminescence imaging. Local, tip-based, near-field, nanoFTIR measurements showed that the photoinduced oxygen vacancy concentration reduction promoted formation of the ferroelectric phase (space group $Pca2_1$) resulting in an increase in the piezoelectric response measured by piezoresponse force microscopy. Photoinduced vacancy tailoring provides, therefore, a spatially prescriptive, post-synthesis, and low-entry method to modify phase in \hfo-based materials.
format Preprint
id arxiv_https___arxiv_org_abs_2406_11763
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Photoinduced Patterning of Oxygen Vacancies to Promote the Ferroelectric Phase of $\mathrm{Hf_{0.5}Zr_{0.5}O_2}$
Beechem, Thomas E
Vega, Fernando
Jaszewski, Samantha T.
Aronson, Benjamin L.
Kelley, Kyle P.
Ihlefeld, Jon F.
Materials Science
Mesoscale and Nanoscale Physics
Photoinduced reductions in the oxygen vacancy concentration were leveraged to increase the ferroelectric phase fraction of $\mathrm{Hf_{0.5}Zr_{0.5}O_2}$ (HZO) thin-films. Modest ($\sim 0.02-0.77~\mathrm{mJ/μm^2}$) laser doses of visible light (488 nm, 2.54 eV) spatially patterned the concentration of oxygen vacancies as monitored by photoluminescence imaging. Local, tip-based, near-field, nanoFTIR measurements showed that the photoinduced oxygen vacancy concentration reduction promoted formation of the ferroelectric phase (space group $Pca2_1$) resulting in an increase in the piezoelectric response measured by piezoresponse force microscopy. Photoinduced vacancy tailoring provides, therefore, a spatially prescriptive, post-synthesis, and low-entry method to modify phase in \hfo-based materials.
title Photoinduced Patterning of Oxygen Vacancies to Promote the Ferroelectric Phase of $\mathrm{Hf_{0.5}Zr_{0.5}O_2}$
topic Materials Science
Mesoscale and Nanoscale Physics
url https://arxiv.org/abs/2406.11763