Point-Spread Function of the Optics in Scanning Electron Microscopes

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Hauptverfasser: Kamal, Surya, Hailstone, Richard K.
Format: Preprint
Veröffentlicht: 2024
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author Kamal, Surya
Hailstone, Richard K.
author_facet Kamal, Surya
Hailstone, Richard K.
contents Point-spread function of the probe forming optics ($PSF_{optics} $) is reported for the first time in an uncorrected (without multipole correctors) scanning electron microscope (SEM). In an SEM, the electron probe information is lost as the beam interacts with the specimen. We show how the probe phase information can be recovered from reconstructed probe intensity estimates. Controlled defocus was used to capture a focal-series of SEM images of $28.5\;nm $ gold ($\mathrm{Au} $) nanoparticles ($\mathrm{NPs} $) on a carbon ($\mathrm C $) film. These images were used to reconstruct their respective probe intensities to create a focal-series of probe intensities, which were the input to the phase retrieval pipeline. Using the complete description (intensity and phase) of the electron probe wavefunction at the specimen plane, we report the $PSF_{optics} $ for multiple data sets for beam energy $E\;=20\;keV\; $. This work opens up new possibilities for an alternative way of aberration correction and aberration-free imaging in scanning electron microscopy.
format Preprint
id arxiv_https___arxiv_org_abs_2407_01439
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Point-Spread Function of the Optics in Scanning Electron Microscopes
Kamal, Surya
Hailstone, Richard K.
Materials Science
Instrumentation and Detectors
Optics
Point-spread function of the probe forming optics ($PSF_{optics} $) is reported for the first time in an uncorrected (without multipole correctors) scanning electron microscope (SEM). In an SEM, the electron probe information is lost as the beam interacts with the specimen. We show how the probe phase information can be recovered from reconstructed probe intensity estimates. Controlled defocus was used to capture a focal-series of SEM images of $28.5\;nm $ gold ($\mathrm{Au} $) nanoparticles ($\mathrm{NPs} $) on a carbon ($\mathrm C $) film. These images were used to reconstruct their respective probe intensities to create a focal-series of probe intensities, which were the input to the phase retrieval pipeline. Using the complete description (intensity and phase) of the electron probe wavefunction at the specimen plane, we report the $PSF_{optics} $ for multiple data sets for beam energy $E\;=20\;keV\; $. This work opens up new possibilities for an alternative way of aberration correction and aberration-free imaging in scanning electron microscopy.
title Point-Spread Function of the Optics in Scanning Electron Microscopes
topic Materials Science
Instrumentation and Detectors
Optics
url https://arxiv.org/abs/2407.01439