Texture tomography with high angular resolution utilizing sparsity

Fuente: arXiv
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Autori principali: Carlsen, Mads, Malamud, Florencia, Modregger, Peter, Wildeis, Anna, Hartmann, Markus, Brandt, Robert, Menzel, Andreas, Liebi, Marianne
Natura: Preprint
Pubblicazione: 2024
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author Carlsen, Mads
Malamud, Florencia
Modregger, Peter
Wildeis, Anna
Hartmann, Markus
Brandt, Robert
Menzel, Andreas
Liebi, Marianne
author_facet Carlsen, Mads
Malamud, Florencia
Modregger, Peter
Wildeis, Anna
Hartmann, Markus
Brandt, Robert
Menzel, Andreas
Liebi, Marianne
contents We demonstrate a novel approach to the reconstruction of scanning probe x-ray diffraction tomography data with anisotropic poly crystalline samples. The method involves reconstructing a voxel map containing an orientation distribution function in each voxel of an extended 3D sample. This method differs from existing approaches by not relying on a peak-finding and is therefore applicable to sample systems consisting of small and highly mosaic crystalline domains that are not handled well by existing methods. Samples of interest include bio-minerals and a range of small-graines microstructures common in engineering metals. By choosing a particular kind of basis functions, we can effectively utilize non-negativity in orientation-space for samples with sparse texture. This enables us to achieve stable solutions at high angular resolutions where the problem would otherwise be under determined. We demonstrate the new approach using data from a shot peened martensite sample where we are able to map the twinning micro structure in the interior of a bulk sample without resolving the individual lattice domains. We also demonstrate the approach on a piece of gastropods shell with a mosaic micro structure.
format Preprint
id arxiv_https___arxiv_org_abs_2407_11022
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Texture tomography with high angular resolution utilizing sparsity
Carlsen, Mads
Malamud, Florencia
Modregger, Peter
Wildeis, Anna
Hartmann, Markus
Brandt, Robert
Menzel, Andreas
Liebi, Marianne
Materials Science
Data Analysis, Statistics and Probability
We demonstrate a novel approach to the reconstruction of scanning probe x-ray diffraction tomography data with anisotropic poly crystalline samples. The method involves reconstructing a voxel map containing an orientation distribution function in each voxel of an extended 3D sample. This method differs from existing approaches by not relying on a peak-finding and is therefore applicable to sample systems consisting of small and highly mosaic crystalline domains that are not handled well by existing methods. Samples of interest include bio-minerals and a range of small-graines microstructures common in engineering metals. By choosing a particular kind of basis functions, we can effectively utilize non-negativity in orientation-space for samples with sparse texture. This enables us to achieve stable solutions at high angular resolutions where the problem would otherwise be under determined. We demonstrate the new approach using data from a shot peened martensite sample where we are able to map the twinning micro structure in the interior of a bulk sample without resolving the individual lattice domains. We also demonstrate the approach on a piece of gastropods shell with a mosaic micro structure.
title Texture tomography with high angular resolution utilizing sparsity
topic Materials Science
Data Analysis, Statistics and Probability
url https://arxiv.org/abs/2407.11022