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Main Authors: Kamble, Shalaka A., Karmakar, Soumen, Bhopale, Somnath R., Jangale, Sanket D., Gadke, Neha P., Ghorui, Srikumar, Bhoraskar, S. V., More, M. A., Mathe, V. L.
Format: Preprint
Published: 2024
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Online Access:https://arxiv.org/abs/2409.06410
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author Kamble, Shalaka A.
Karmakar, Soumen
Bhopale, Somnath R.
Jangale, Sanket D.
Gadke, Neha P.
Ghorui, Srikumar
Bhoraskar, S. V.
More, M. A.
Mathe, V. L.
author_facet Kamble, Shalaka A.
Karmakar, Soumen
Bhopale, Somnath R.
Jangale, Sanket D.
Gadke, Neha P.
Ghorui, Srikumar
Bhoraskar, S. V.
More, M. A.
Mathe, V. L.
contents Herein, we report a case study in which we saw the spontaneous conversion of commercial bulk graphite into LaB6 decorated carbon nanotubes (CNTs) under normal atmospheric conditions. The feedstock graphite was used as a hollow cylindrical anode filled with LaB6 powder and partially eroded in a DC electric-arc plasma reactor in pure nitrogen atmosphere. An unusual and spontaneous deformation of the plasma-treated residual anode into a fluffy powder was seen to continue for months when left to ambient atmospheric conditions. The existence of LaB6 decorated multi-walled CNTs at large quantity was confirmed in the as-generated powder by using electron microscopy, Raman spectroscopy and x-ray diffraction. The as-synthesized CNT-based large-area field emitter showed promising field-emitting properties with a low turn-on electric field of ~1.5 V per micrometer, and a current density of ~1.17 mA per square cm at an applied electric field of 3.24 V per micrometer.
format Preprint
id arxiv_https___arxiv_org_abs_2409_06410
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle LaB6 aided spontaneous conversion of bulk graphite into carbon nanotubes at normal atmospheric conditions
Kamble, Shalaka A.
Karmakar, Soumen
Bhopale, Somnath R.
Jangale, Sanket D.
Gadke, Neha P.
Ghorui, Srikumar
Bhoraskar, S. V.
More, M. A.
Mathe, V. L.
Materials Science
Applied Physics
Herein, we report a case study in which we saw the spontaneous conversion of commercial bulk graphite into LaB6 decorated carbon nanotubes (CNTs) under normal atmospheric conditions. The feedstock graphite was used as a hollow cylindrical anode filled with LaB6 powder and partially eroded in a DC electric-arc plasma reactor in pure nitrogen atmosphere. An unusual and spontaneous deformation of the plasma-treated residual anode into a fluffy powder was seen to continue for months when left to ambient atmospheric conditions. The existence of LaB6 decorated multi-walled CNTs at large quantity was confirmed in the as-generated powder by using electron microscopy, Raman spectroscopy and x-ray diffraction. The as-synthesized CNT-based large-area field emitter showed promising field-emitting properties with a low turn-on electric field of ~1.5 V per micrometer, and a current density of ~1.17 mA per square cm at an applied electric field of 3.24 V per micrometer.
title LaB6 aided spontaneous conversion of bulk graphite into carbon nanotubes at normal atmospheric conditions
topic Materials Science
Applied Physics
url https://arxiv.org/abs/2409.06410