Effect of Grafting Density on the Two-dimensional Assembly of Nanoparticles

Fuente: arXiv
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Hauptverfasser: Nayak, Binay P., Batey, James Ethan, Kim, Hyeong Jin, Wang, Wenjie, Bu, Wei, Zhang, Honghu, Mallapragada, Surya K., Vaknin, David
Format: Preprint
Veröffentlicht: 2024
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author Nayak, Binay P.
Batey, James Ethan
Kim, Hyeong Jin
Wang, Wenjie
Bu, Wei
Zhang, Honghu
Mallapragada, Surya K.
Vaknin, David
author_facet Nayak, Binay P.
Batey, James Ethan
Kim, Hyeong Jin
Wang, Wenjie
Bu, Wei
Zhang, Honghu
Mallapragada, Surya K.
Vaknin, David
contents Employing grazing-incidence small-angle X-ray scattering (GISAXS) and X-ray reflectivity (XRR), we demonstrate that films composed of polyethylene glycol (PEG)-grafted silver nanoparticles (AgNP) and gold nanoparticles (AuNP), as well as their binary mixtures, form highly stable hexagonal structures at the vapor-liquid interface. These nanoparticles exhibit remarkable stability under varying environmental conditions, including changes in pH, mixing concentration, and PEG chain length. Short-chain PEG grafting produces dense, well-ordered films, while longer chains produce more complex, less dense quasi-bilayer structures. AuNPs exhibit higher grafting densities than AgNPs, leading to more ordered in-plane arrangements. In binary mixtures, AuNPs dominate the population at the surface, while AgNPs integrate into the system, expanding the lattice without forming a distinct binary superstructure. These results offer valuable insights into the structural behavior of PEG-grafted nanoparticles and provide a foundation for optimizing binary nanoparticle assemblies for advanced nanotechnology applications.
format Preprint
id arxiv_https___arxiv_org_abs_2410_05456
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Effect of Grafting Density on the Two-dimensional Assembly of Nanoparticles
Nayak, Binay P.
Batey, James Ethan
Kim, Hyeong Jin
Wang, Wenjie
Bu, Wei
Zhang, Honghu
Mallapragada, Surya K.
Vaknin, David
Soft Condensed Matter
Employing grazing-incidence small-angle X-ray scattering (GISAXS) and X-ray reflectivity (XRR), we demonstrate that films composed of polyethylene glycol (PEG)-grafted silver nanoparticles (AgNP) and gold nanoparticles (AuNP), as well as their binary mixtures, form highly stable hexagonal structures at the vapor-liquid interface. These nanoparticles exhibit remarkable stability under varying environmental conditions, including changes in pH, mixing concentration, and PEG chain length. Short-chain PEG grafting produces dense, well-ordered films, while longer chains produce more complex, less dense quasi-bilayer structures. AuNPs exhibit higher grafting densities than AgNPs, leading to more ordered in-plane arrangements. In binary mixtures, AuNPs dominate the population at the surface, while AgNPs integrate into the system, expanding the lattice without forming a distinct binary superstructure. These results offer valuable insights into the structural behavior of PEG-grafted nanoparticles and provide a foundation for optimizing binary nanoparticle assemblies for advanced nanotechnology applications.
title Effect of Grafting Density on the Two-dimensional Assembly of Nanoparticles
topic Soft Condensed Matter
url https://arxiv.org/abs/2410.05456