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Main Authors: Kundu, Anirban, Jalali, Seyed Kamal, Kim, Minhyeok, Wang, Meihui, Luo, Da, Lee, Sun Hwa, Pugno, Nicola M., Seong, Won Kyung, Ruoff, Rodney S.
Format: Preprint
Published: 2024
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Online Access:https://arxiv.org/abs/2411.01440
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author Kundu, Anirban
Jalali, Seyed Kamal
Kim, Minhyeok
Wang, Meihui
Luo, Da
Lee, Sun Hwa
Pugno, Nicola M.
Seong, Won Kyung
Ruoff, Rodney S.
author_facet Kundu, Anirban
Jalali, Seyed Kamal
Kim, Minhyeok
Wang, Meihui
Luo, Da
Lee, Sun Hwa
Pugno, Nicola M.
Seong, Won Kyung
Ruoff, Rodney S.
contents Despite extensive microscale studies, the macroscopic mechanical properties of monolayer graphene remain underexplored. Here, we report the Young's modulus ($E$ = 1.11 $\pm$ 0.04 TPa), tensile strength ($σ$ = 27.40 $\pm$ 4.36 GPa), and failure strain ($ε_f$ = 6.01 $\pm$ 0.92 %) of centimeter-scale single-crystal monolayer graphene (SCG) 'dog bone' samples with edges aligned along the zigzag (zz) direction, supported by an ultra-thin polymer (polycarbonate) film. For samples with edges along the armchair (ac) direction, we obtain $E$ = 1.01 $\pm$ 0.10 TPa, $σ$ = 20.21 $\pm$ 3.22 GPa, $ε_f$ = 3.69 $\pm$ 0.38 %, and for chiral samples whose edges were between zz and ac, we obtain $E$= 0.75 $\pm$ 0.12 TPa, $σ$ = 23.56 $\pm$ 3.42 GPa, and $ε_f$ = 4.53 $\pm$ 0.40 %. The SCG is grown on single crystal Cu(111) foils by chemical vapor deposition (CVD). We used a home-built 'float-on-water' (FOW) tensile testing system for tensile loading measurements that also enabled in situ crack observation. The quantized fracture mechanics (QFM) analysis predicts an edge defect size from several to tens of nanometers based on chirality and notch angle. Through Weibull analysis and given that the fatal defects are confined on the edges of macroscale samples, we projected strength ranging from 13.67 to 18.43 GPa for an A4-size SCG according to their chirality. The exceptional mechanical performance of macroscale single crystal graphene (SCG) paves the way for its widespread use in a very wide variety of applications.
format Preprint
id arxiv_https___arxiv_org_abs_2411_01440
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle The Mechanical Behavior of Macroscale Single-crystal Graphene
Kundu, Anirban
Jalali, Seyed Kamal
Kim, Minhyeok
Wang, Meihui
Luo, Da
Lee, Sun Hwa
Pugno, Nicola M.
Seong, Won Kyung
Ruoff, Rodney S.
Mesoscale and Nanoscale Physics
Materials Science
Despite extensive microscale studies, the macroscopic mechanical properties of monolayer graphene remain underexplored. Here, we report the Young's modulus ($E$ = 1.11 $\pm$ 0.04 TPa), tensile strength ($σ$ = 27.40 $\pm$ 4.36 GPa), and failure strain ($ε_f$ = 6.01 $\pm$ 0.92 %) of centimeter-scale single-crystal monolayer graphene (SCG) 'dog bone' samples with edges aligned along the zigzag (zz) direction, supported by an ultra-thin polymer (polycarbonate) film. For samples with edges along the armchair (ac) direction, we obtain $E$ = 1.01 $\pm$ 0.10 TPa, $σ$ = 20.21 $\pm$ 3.22 GPa, $ε_f$ = 3.69 $\pm$ 0.38 %, and for chiral samples whose edges were between zz and ac, we obtain $E$= 0.75 $\pm$ 0.12 TPa, $σ$ = 23.56 $\pm$ 3.42 GPa, and $ε_f$ = 4.53 $\pm$ 0.40 %. The SCG is grown on single crystal Cu(111) foils by chemical vapor deposition (CVD). We used a home-built 'float-on-water' (FOW) tensile testing system for tensile loading measurements that also enabled in situ crack observation. The quantized fracture mechanics (QFM) analysis predicts an edge defect size from several to tens of nanometers based on chirality and notch angle. Through Weibull analysis and given that the fatal defects are confined on the edges of macroscale samples, we projected strength ranging from 13.67 to 18.43 GPa for an A4-size SCG according to their chirality. The exceptional mechanical performance of macroscale single crystal graphene (SCG) paves the way for its widespread use in a very wide variety of applications.
title The Mechanical Behavior of Macroscale Single-crystal Graphene
topic Mesoscale and Nanoscale Physics
Materials Science
url https://arxiv.org/abs/2411.01440