Radical-mediated Electrical Enzyme Assay For At-home Clinical Test

Fuente: arXiv
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Autori principali: Jang, Hyun-June, Joung, Hyou-Arm, Shi, Xiaoao, Ding, Rui, Wagner, Justine, Tang, Erting, Zhuang, Wen, Ryu, Byunghoon, Chen, Guanmin, Yeo, Kiang-Teck Jerry, Huang, Jun, Chen, Junhong
Natura: Preprint
Pubblicazione: 2024
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author Jang, Hyun-June
Joung, Hyou-Arm
Shi, Xiaoao
Ding, Rui
Wagner, Justine
Tang, Erting
Zhuang, Wen
Ryu, Byunghoon
Chen, Guanmin
Yeo, Kiang-Teck Jerry
Huang, Jun
Chen, Junhong
author_facet Jang, Hyun-June
Joung, Hyou-Arm
Shi, Xiaoao
Ding, Rui
Wagner, Justine
Tang, Erting
Zhuang, Wen
Ryu, Byunghoon
Chen, Guanmin
Yeo, Kiang-Teck Jerry
Huang, Jun
Chen, Junhong
contents To meet the growing demand for accurate, rapid, and cost-effective at-home clinical testing, we developed a radical-mediated enzyme assay (REEA) integrated with a paper fluidic system and electrically read by a handheld field-effect transistor (FET) device. The REEA utilizes horseradish peroxidase (HRP) to catalyze the conversion of aromatic substrates into radical forms, producing protons detected by an ion-sensitive FET for biomarker quantification. Through screening 14 phenolic compounds, halogenated phenols emerged as optimal substrates for the REEA. Encased in an affordable cartridge ($0.55 per test), the system achieved a detection limit of 146 fg/mL for estradiol (E2), with a coefficient of variation (CV) below 9.2% in E2-spiked samples and an r2 of 0.963 across a measuring range of 19 to 4,551 pg/mL in clinical plasma samples, providing results in under 10 minutes. This adaptable system not only promises to offer a fast and reliable platform, but also holds significant potential for expansion to a wide array of biomarkers, paving the way for broader clinical and home-based applications.
format Preprint
id arxiv_https___arxiv_org_abs_2411_03111
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Radical-mediated Electrical Enzyme Assay For At-home Clinical Test
Jang, Hyun-June
Joung, Hyou-Arm
Shi, Xiaoao
Ding, Rui
Wagner, Justine
Tang, Erting
Zhuang, Wen
Ryu, Byunghoon
Chen, Guanmin
Yeo, Kiang-Teck Jerry
Huang, Jun
Chen, Junhong
Quantitative Methods
To meet the growing demand for accurate, rapid, and cost-effective at-home clinical testing, we developed a radical-mediated enzyme assay (REEA) integrated with a paper fluidic system and electrically read by a handheld field-effect transistor (FET) device. The REEA utilizes horseradish peroxidase (HRP) to catalyze the conversion of aromatic substrates into radical forms, producing protons detected by an ion-sensitive FET for biomarker quantification. Through screening 14 phenolic compounds, halogenated phenols emerged as optimal substrates for the REEA. Encased in an affordable cartridge ($0.55 per test), the system achieved a detection limit of 146 fg/mL for estradiol (E2), with a coefficient of variation (CV) below 9.2% in E2-spiked samples and an r2 of 0.963 across a measuring range of 19 to 4,551 pg/mL in clinical plasma samples, providing results in under 10 minutes. This adaptable system not only promises to offer a fast and reliable platform, but also holds significant potential for expansion to a wide array of biomarkers, paving the way for broader clinical and home-based applications.
title Radical-mediated Electrical Enzyme Assay For At-home Clinical Test
topic Quantitative Methods
url https://arxiv.org/abs/2411.03111