Detection of Sulfur Dioxide by Broadband Cavity-Enhanced Absorption Spectroscopy (BBCEAS)

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Main Authors: Thalman, Ryan, Bhardwaj, Nitish, Flowerday, Callum E., Hansen, Jaron C.
Format: Preprint
Published: 2024
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author Thalman, Ryan
Bhardwaj, Nitish
Flowerday, Callum E.
Hansen, Jaron C.
author_facet Thalman, Ryan
Bhardwaj, Nitish
Flowerday, Callum E.
Hansen, Jaron C.
contents Sulfur dioxide ($\mathrm{SO}_2$) is an important precursor for the formation of atmospheric sulfate aerosol and acid rain. We present an instrument using Broadband Cavity-Enhanced Absorption Spectroscopy (BBCEAS) for the measurement of $\mathrm{SO}_2$ with a minimum limit of detection of 0.75 ppbv (3-$σ$) using the spectral range 305.5--312 nm and an averaging time of 5 min. The instrument consists of high-reflectivity mirrors (0.9985 at 310 nm) and a deep UV light source (Light Emitting Diode). The effective absorption path length of the instrument is 610 m with a 0.966 m base length. Published reference absorption cross sections were used to fit and retrieve the $\mathrm{SO}_2$ concentrations and were compared to fluorescence standard measurements for $\mathrm{SO}_2$. The comparison was well correlated ($R^2 = 0.9998$) with a correlation slope of 1.04. Interferences for fluorescence measurements were tested, and the BBCEAS showed no interference, while ambient measurements responded similarly to standard measurement techniques.
format Preprint
id arxiv_https___arxiv_org_abs_2411_15601
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Detection of Sulfur Dioxide by Broadband Cavity-Enhanced Absorption Spectroscopy (BBCEAS)
Thalman, Ryan
Bhardwaj, Nitish
Flowerday, Callum E.
Hansen, Jaron C.
Instrumentation and Detectors
Atmospheric and Oceanic Physics
Sulfur dioxide ($\mathrm{SO}_2$) is an important precursor for the formation of atmospheric sulfate aerosol and acid rain. We present an instrument using Broadband Cavity-Enhanced Absorption Spectroscopy (BBCEAS) for the measurement of $\mathrm{SO}_2$ with a minimum limit of detection of 0.75 ppbv (3-$σ$) using the spectral range 305.5--312 nm and an averaging time of 5 min. The instrument consists of high-reflectivity mirrors (0.9985 at 310 nm) and a deep UV light source (Light Emitting Diode). The effective absorption path length of the instrument is 610 m with a 0.966 m base length. Published reference absorption cross sections were used to fit and retrieve the $\mathrm{SO}_2$ concentrations and were compared to fluorescence standard measurements for $\mathrm{SO}_2$. The comparison was well correlated ($R^2 = 0.9998$) with a correlation slope of 1.04. Interferences for fluorescence measurements were tested, and the BBCEAS showed no interference, while ambient measurements responded similarly to standard measurement techniques.
title Detection of Sulfur Dioxide by Broadband Cavity-Enhanced Absorption Spectroscopy (BBCEAS)
topic Instrumentation and Detectors
Atmospheric and Oceanic Physics
url https://arxiv.org/abs/2411.15601