Transmission of radio-frequency waves and nuclear magnetic resonance in lanthanum superhydrides

Fuente: arXiv
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Main Authors: Semenok, Dmitrii V., Bärtl, Florian, Zhou, Di, Helm, Toni, Luther, Sven, Kühne, Hannes, Wosnitza, J., Troyan, Ivan A., Struzhkin, Viktor V.
Format: Preprint
Published: 2024
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author Semenok, Dmitrii V.
Bärtl, Florian
Zhou, Di
Helm, Toni
Luther, Sven
Kühne, Hannes
Wosnitza, J.
Troyan, Ivan A.
Struzhkin, Viktor V.
author_facet Semenok, Dmitrii V.
Bärtl, Florian
Zhou, Di
Helm, Toni
Luther, Sven
Kühne, Hannes
Wosnitza, J.
Troyan, Ivan A.
Struzhkin, Viktor V.
contents The discovery of near-room temperature superconductivity in the lanthanum hydride LaH$_{10}$ has revolutionized this field of research. However, the need to use diamond anvils for the synthesis of such superconductors severely limits the number of experimental techniques to study these materials. Nuclear magnetic resonance (NMR) is one of the key methods for probing spin systems of superconductors. In this work, we show how $^1$H NMR measurements can be realized in diamond anvil cells to study high-temperature superconductivity in lanthanum polyhydrides at pressures up to 165 GPa. In the newly discovered superhydride LaH$_{12}$, we observed a pronounced suppression of the $^1$H NMR signal intensity below $\textit{T$_{c}$(onset)}$ = 260 K in a magnetic field of 7 T, corresponding to the screening of the radio-frequency pulses. Below the critical temperature of superconductivity, all $^1$H NMR characteristics, including the spin-lattice relaxation rate $\textit{1/T$_{1}$T}$, demonstrate pronounced features, evidencing the bulk nature of the superconducting transition. In zero field, the radio-frequency signal transmission through the LaH$_{12}$ sample shows a pronounced drop below $\textit{T$_{c}$(onset)}$ = 267 K, confirming the superconducting nature of the transition. A description of the $\textit{1/T$_{1}$T}$ data with an exponential form allows the estimation of the superconducting gap $\textit{$Δ$(0)}$ lying between 427 and 671 K (corresponding to 36.8 to 57.8 meV), and the ratio $\textit{R$_Δ$ = 2$Δ$(0)/k$_B$T$_c$}$ between 3.76 and 5.16 in the synthesized hydride sample.
format Preprint
id arxiv_https___arxiv_org_abs_2412_11727
institution arXiv
publishDate 2024
record_format arxiv
spellingShingle Transmission of radio-frequency waves and nuclear magnetic resonance in lanthanum superhydrides
Semenok, Dmitrii V.
Bärtl, Florian
Zhou, Di
Helm, Toni
Luther, Sven
Kühne, Hannes
Wosnitza, J.
Troyan, Ivan A.
Struzhkin, Viktor V.
Superconductivity
Materials Science
The discovery of near-room temperature superconductivity in the lanthanum hydride LaH$_{10}$ has revolutionized this field of research. However, the need to use diamond anvils for the synthesis of such superconductors severely limits the number of experimental techniques to study these materials. Nuclear magnetic resonance (NMR) is one of the key methods for probing spin systems of superconductors. In this work, we show how $^1$H NMR measurements can be realized in diamond anvil cells to study high-temperature superconductivity in lanthanum polyhydrides at pressures up to 165 GPa. In the newly discovered superhydride LaH$_{12}$, we observed a pronounced suppression of the $^1$H NMR signal intensity below $\textit{T$_{c}$(onset)}$ = 260 K in a magnetic field of 7 T, corresponding to the screening of the radio-frequency pulses. Below the critical temperature of superconductivity, all $^1$H NMR characteristics, including the spin-lattice relaxation rate $\textit{1/T$_{1}$T}$, demonstrate pronounced features, evidencing the bulk nature of the superconducting transition. In zero field, the radio-frequency signal transmission through the LaH$_{12}$ sample shows a pronounced drop below $\textit{T$_{c}$(onset)}$ = 267 K, confirming the superconducting nature of the transition. A description of the $\textit{1/T$_{1}$T}$ data with an exponential form allows the estimation of the superconducting gap $\textit{$Δ$(0)}$ lying between 427 and 671 K (corresponding to 36.8 to 57.8 meV), and the ratio $\textit{R$_Δ$ = 2$Δ$(0)/k$_B$T$_c$}$ between 3.76 and 5.16 in the synthesized hydride sample.
title Transmission of radio-frequency waves and nuclear magnetic resonance in lanthanum superhydrides
topic Superconductivity
Materials Science
url https://arxiv.org/abs/2412.11727