Absence of superconductivity and density-wave transition in ambient-pressure tetragonal La$_4$Ni$_3$O$_{10}$

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Hauptverfasser: Shi, Mengzhu, Li, Yikang, Wang, Yuxing, Peng, Di, Yang, Shaohua, Li, Houpu, Fan, Kaibao, Jiang, Kun, He, Junfeng, Zeng, Qiaoshi, Song, Dongsheng, Ge, Binghui, Xiang, Ziji, Wang, Zhenyu, Ying, Jianjun, Wu, Tao, Chen, Xianhui
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Veröffentlicht: 2025
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author Shi, Mengzhu
Li, Yikang
Wang, Yuxing
Peng, Di
Yang, Shaohua
Li, Houpu
Fan, Kaibao
Jiang, Kun
He, Junfeng
Zeng, Qiaoshi
Song, Dongsheng
Ge, Binghui
Xiang, Ziji
Wang, Zhenyu
Ying, Jianjun
Wu, Tao
Chen, Xianhui
author_facet Shi, Mengzhu
Li, Yikang
Wang, Yuxing
Peng, Di
Yang, Shaohua
Li, Houpu
Fan, Kaibao
Jiang, Kun
He, Junfeng
Zeng, Qiaoshi
Song, Dongsheng
Ge, Binghui
Xiang, Ziji
Wang, Zhenyu
Ying, Jianjun
Wu, Tao
Chen, Xianhui
contents The recent discovery of superconductivity in La$_3$Ni$_2$O$_7$ and La$_4$Ni$_3$O$_{10}$ under high pressure stimulates intensive research interests. These nickelates crystallize in an orthogonal/monoclinic structure with tilted NiO$_6$ octahedra at ambient pressure and enter a density-wave-like phase at low temperatures. The application of pressure suppresses the octahedral tilting and triggers a transition to tetragonal structure (I4/mmm), which is believed to be a key prerequisite for the emergence of superconducting state. Here, by developing a high oxidative environment growth technology, we report the first tetragonal nickelates La$_4$Ni$_3$O$_{10}$ microcrystals without octahedral tilting at ambient pressure. In tetragonal La$_4$Ni$_3$O$_{10}$, transport measurements find that both density-wave and superconducting transitions are absent up to 160 GPa, indicating a robust tetragonal metallic ground state. Density functional theory calculations reveal that the band structure of ambient-pressure tetragonal La$_4$Ni$_3$O$_{10}$ involves more $d_{z2}$ orbital contribution to the Fermi surface, compared to the monoclinic phase or the high-pressure superconducting tetragonal phase. The concurrent absence of density-wave state and high-pressure superconductivity in our ambient-pressure tetragonal crystals of La$_4$Ni$_3$O$_{10}$ suggests an underlying correlation between these two orders. It suggests that the tetragonal structure is not necessary, while the density-wave state is crucial for the superconductivity in nickelates. Our findings impose important constraints on the mechanism of pressure-induced superconductivity in nickelates and sheds new light on exploring ambient pressure high-temperature Ni-based superconductors.
format Preprint
id arxiv_https___arxiv_org_abs_2501_12647
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Absence of superconductivity and density-wave transition in ambient-pressure tetragonal La$_4$Ni$_3$O$_{10}$
Shi, Mengzhu
Li, Yikang
Wang, Yuxing
Peng, Di
Yang, Shaohua
Li, Houpu
Fan, Kaibao
Jiang, Kun
He, Junfeng
Zeng, Qiaoshi
Song, Dongsheng
Ge, Binghui
Xiang, Ziji
Wang, Zhenyu
Ying, Jianjun
Wu, Tao
Chen, Xianhui
Superconductivity
Materials Science
The recent discovery of superconductivity in La$_3$Ni$_2$O$_7$ and La$_4$Ni$_3$O$_{10}$ under high pressure stimulates intensive research interests. These nickelates crystallize in an orthogonal/monoclinic structure with tilted NiO$_6$ octahedra at ambient pressure and enter a density-wave-like phase at low temperatures. The application of pressure suppresses the octahedral tilting and triggers a transition to tetragonal structure (I4/mmm), which is believed to be a key prerequisite for the emergence of superconducting state. Here, by developing a high oxidative environment growth technology, we report the first tetragonal nickelates La$_4$Ni$_3$O$_{10}$ microcrystals without octahedral tilting at ambient pressure. In tetragonal La$_4$Ni$_3$O$_{10}$, transport measurements find that both density-wave and superconducting transitions are absent up to 160 GPa, indicating a robust tetragonal metallic ground state. Density functional theory calculations reveal that the band structure of ambient-pressure tetragonal La$_4$Ni$_3$O$_{10}$ involves more $d_{z2}$ orbital contribution to the Fermi surface, compared to the monoclinic phase or the high-pressure superconducting tetragonal phase. The concurrent absence of density-wave state and high-pressure superconductivity in our ambient-pressure tetragonal crystals of La$_4$Ni$_3$O$_{10}$ suggests an underlying correlation between these two orders. It suggests that the tetragonal structure is not necessary, while the density-wave state is crucial for the superconductivity in nickelates. Our findings impose important constraints on the mechanism of pressure-induced superconductivity in nickelates and sheds new light on exploring ambient pressure high-temperature Ni-based superconductors.
title Absence of superconductivity and density-wave transition in ambient-pressure tetragonal La$_4$Ni$_3$O$_{10}$
topic Superconductivity
Materials Science
url https://arxiv.org/abs/2501.12647