Ultimate Sensitivity in X-ray Diffraction: Angular Moments vs. Shot Noise

Fuente: arXiv
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Autori principali: Modregger, Peter, Wittwer, Felix, Khaliq, Ahmar, Pyrlik, Niklas, Ball, James A. D., Garrevoet, Jan, Falkenberg, Gerald, Liehr, Alexander, Stuckelberger, Michael
Natura: Preprint
Pubblicazione: 2025
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author Modregger, Peter
Wittwer, Felix
Khaliq, Ahmar
Pyrlik, Niklas
Ball, James A. D.
Garrevoet, Jan
Falkenberg, Gerald
Liehr, Alexander
Stuckelberger, Michael
author_facet Modregger, Peter
Wittwer, Felix
Khaliq, Ahmar
Pyrlik, Niklas
Ball, James A. D.
Garrevoet, Jan
Falkenberg, Gerald
Liehr, Alexander
Stuckelberger, Michael
contents The sensitivity of x-ray diffraction experiments towards Bragg peak parameters constitutes a crucial performance attribute of experimental setups. Frequently, diffraction peaks are characterized by model-free angular moment analysis, which offers a greater versatility compared to traditional model-based peak fitting. Here, we have determined the ultimate sensitivity of angular moments for diffraction data that is limited by photon shot noise. We report experimentally achieved sensitivities of the first moment below $1/1000$th of a detector pixel and below $1μ$rad. We have demonstrated the validity of our theoretical predictions by an excellent agreement with experimental results from three different setups. The provided formulas for the uncertainties of angular moments allow for the rapid determination of experimentally achieved sensitivities from single diffraction frames.
format Preprint
id arxiv_https___arxiv_org_abs_2502_17977
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Ultimate Sensitivity in X-ray Diffraction: Angular Moments vs. Shot Noise
Modregger, Peter
Wittwer, Felix
Khaliq, Ahmar
Pyrlik, Niklas
Ball, James A. D.
Garrevoet, Jan
Falkenberg, Gerald
Liehr, Alexander
Stuckelberger, Michael
Optics
Data Analysis, Statistics and Probability
The sensitivity of x-ray diffraction experiments towards Bragg peak parameters constitutes a crucial performance attribute of experimental setups. Frequently, diffraction peaks are characterized by model-free angular moment analysis, which offers a greater versatility compared to traditional model-based peak fitting. Here, we have determined the ultimate sensitivity of angular moments for diffraction data that is limited by photon shot noise. We report experimentally achieved sensitivities of the first moment below $1/1000$th of a detector pixel and below $1μ$rad. We have demonstrated the validity of our theoretical predictions by an excellent agreement with experimental results from three different setups. The provided formulas for the uncertainties of angular moments allow for the rapid determination of experimentally achieved sensitivities from single diffraction frames.
title Ultimate Sensitivity in X-ray Diffraction: Angular Moments vs. Shot Noise
topic Optics
Data Analysis, Statistics and Probability
url https://arxiv.org/abs/2502.17977