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Main Authors: Khardazi, S., Mezzane, D., Amjoud, M., Novak, N., Choukri, E., Lyubchyk, S., Kutnjak, Z., Rožič, B., Terenchuk, S., Lukyanchuk, I.
Format: Preprint
Published: 2025
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Online Access:https://arxiv.org/abs/2503.08519
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author Khardazi, S.
Mezzane, D.
Amjoud, M.
Novak, N.
Choukri, E.
Lyubchyk, S.
Kutnjak, Z.
Rožič, B.
Terenchuk, S.
Lukyanchuk, I.
author_facet Khardazi, S.
Mezzane, D.
Amjoud, M.
Novak, N.
Choukri, E.
Lyubchyk, S.
Kutnjak, Z.
Rožič, B.
Terenchuk, S.
Lukyanchuk, I.
contents Lead-free perovskite ceramics Ba(1-x)LaxTi0.89Sn0.11O3 with x= 0, 0.015, 0.025, and 0.035 (BLTSnx) were synthesized by solid-state reaction method. The enhanced energy storage properties were studied across the ferroelectric relaxor conversion. The pure perovskite structure of all prepared samples was confirmed by X-ray diffraction (XRD) analysis and the Raman spectroscopy technique. Scanning electron microscopy micrographs show a drastic decrease in the grain size in La-doped ceramics. Furthermore, the doped samples exhibit smeared phase transition and frequency dispersion in dielectric permittivity, typical for relaxors. The P-E hysteresis loops become thin with the increase of the La-doping, demonstrating the ferroelectric-relaxor phase conversion. The enhanced recovered energy density and the energy storage efficiency of 158.8 mJ/cm3 and 82.73 % were observed in the BLTSn2.5 sample at room temperature, respectively. These properties indicate that environmentally friendly BLTSn2.5 is a viable candidate for energy-storage capacitor applications near room temperature.
format Preprint
id arxiv_https___arxiv_org_abs_2503_08519
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Improved thermal stability of dielectric properties and energy storage properties of lead-free relaxor Ba(1-x)LaxTi0.89Sn0.11O3 ceramics
Khardazi, S.
Mezzane, D.
Amjoud, M.
Novak, N.
Choukri, E.
Lyubchyk, S.
Kutnjak, Z.
Rožič, B.
Terenchuk, S.
Lukyanchuk, I.
Materials Science
Lead-free perovskite ceramics Ba(1-x)LaxTi0.89Sn0.11O3 with x= 0, 0.015, 0.025, and 0.035 (BLTSnx) were synthesized by solid-state reaction method. The enhanced energy storage properties were studied across the ferroelectric relaxor conversion. The pure perovskite structure of all prepared samples was confirmed by X-ray diffraction (XRD) analysis and the Raman spectroscopy technique. Scanning electron microscopy micrographs show a drastic decrease in the grain size in La-doped ceramics. Furthermore, the doped samples exhibit smeared phase transition and frequency dispersion in dielectric permittivity, typical for relaxors. The P-E hysteresis loops become thin with the increase of the La-doping, demonstrating the ferroelectric-relaxor phase conversion. The enhanced recovered energy density and the energy storage efficiency of 158.8 mJ/cm3 and 82.73 % were observed in the BLTSn2.5 sample at room temperature, respectively. These properties indicate that environmentally friendly BLTSn2.5 is a viable candidate for energy-storage capacitor applications near room temperature.
title Improved thermal stability of dielectric properties and energy storage properties of lead-free relaxor Ba(1-x)LaxTi0.89Sn0.11O3 ceramics
topic Materials Science
url https://arxiv.org/abs/2503.08519