Growth of Highly Conductive PtSe2 Films Controlled by Raman Metrics for High-Frequency Photodetectors and Optoelectronic Mixers at 1.55 μm

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Main Authors: Desgué, Eva, Verschueren, Ivan, Tharrault, Marin, Dosenovic, Djordje, Largeau, Ludovic, Grimaldi, Eva, Pommier, Delphine, Jussey, Doriane, Moreau, Bérangère, Carisetti, Dominique, Gangloff, Laurent, Plouhinec, Patrick, Messudom, Naomie, Bouyid, Zineb, Pribat, Didier, Chaste, Julien, Ouerghi, Abdelkarim, Plaçais, Bernard, Baudin, Emmanuel, Okuno, Hanako, Legagneux, Pierre
Format: Preprint
Published: 2025
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_version_ 1866915299720167424
author Desgué, Eva
Verschueren, Ivan
Tharrault, Marin
Dosenovic, Djordje
Largeau, Ludovic
Grimaldi, Eva
Pommier, Delphine
Jussey, Doriane
Moreau, Bérangère
Carisetti, Dominique
Gangloff, Laurent
Plouhinec, Patrick
Messudom, Naomie
Bouyid, Zineb
Pribat, Didier
Chaste, Julien
Ouerghi, Abdelkarim
Plaçais, Bernard
Baudin, Emmanuel
Okuno, Hanako
Legagneux, Pierre
author_facet Desgué, Eva
Verschueren, Ivan
Tharrault, Marin
Dosenovic, Djordje
Largeau, Ludovic
Grimaldi, Eva
Pommier, Delphine
Jussey, Doriane
Moreau, Bérangère
Carisetti, Dominique
Gangloff, Laurent
Plouhinec, Patrick
Messudom, Naomie
Bouyid, Zineb
Pribat, Didier
Chaste, Julien
Ouerghi, Abdelkarim
Plaçais, Bernard
Baudin, Emmanuel
Okuno, Hanako
Legagneux, Pierre
contents Two-dimensional PtSe2 exhibits outstanding intrinsic properties such as high carrier mobility, tunable bandgap, broadband absorption and air stability, making it ideal for (opto)electronic applications. However, achieving films of high crystalline quality with controlled properties on low-cost and insulating substrates remains challenging. Here, highly crystalline semimetallic PtSe2 films are grown by molecular beam epitaxy on sapphire substrates. It is shown that a post-growth annealing remarkably improves the out-of-plane crystallinity and leads to record sheet conductances, up to 1.6 mS. In-depth structural analyses reveal the strong influence of the domain arrangement within the films on their sheet conductance. Moreover, it is demonstrated that the A1g Raman peak width, in addition to the commonly used Eg peak width, are both effective metrics for evaluating the quality of PtSe2: films with narrower Eg and A1g peaks exhibit higher in-plane and out-of-plane crystalline quality, as well as higher sheet conductance. Finally, coplanar waveguides integrating a semimetallic PtSe2 channel are fabricated on a 2-inch sapphire substrate to demonstrate optoelectronic devices operating at the 1.55 um telecom wavelength. This includes photodetectors with a record bandwidth of 60 GHz and the first PtSe2-based optoelectronic mixer with a 30 GHz bandwidth.
format Preprint
id arxiv_https___arxiv_org_abs_2503_20659
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Growth of Highly Conductive PtSe2 Films Controlled by Raman Metrics for High-Frequency Photodetectors and Optoelectronic Mixers at 1.55 μm
Desgué, Eva
Verschueren, Ivan
Tharrault, Marin
Dosenovic, Djordje
Largeau, Ludovic
Grimaldi, Eva
Pommier, Delphine
Jussey, Doriane
Moreau, Bérangère
Carisetti, Dominique
Gangloff, Laurent
Plouhinec, Patrick
Messudom, Naomie
Bouyid, Zineb
Pribat, Didier
Chaste, Julien
Ouerghi, Abdelkarim
Plaçais, Bernard
Baudin, Emmanuel
Okuno, Hanako
Legagneux, Pierre
Materials Science
Applied Physics
Two-dimensional PtSe2 exhibits outstanding intrinsic properties such as high carrier mobility, tunable bandgap, broadband absorption and air stability, making it ideal for (opto)electronic applications. However, achieving films of high crystalline quality with controlled properties on low-cost and insulating substrates remains challenging. Here, highly crystalline semimetallic PtSe2 films are grown by molecular beam epitaxy on sapphire substrates. It is shown that a post-growth annealing remarkably improves the out-of-plane crystallinity and leads to record sheet conductances, up to 1.6 mS. In-depth structural analyses reveal the strong influence of the domain arrangement within the films on their sheet conductance. Moreover, it is demonstrated that the A1g Raman peak width, in addition to the commonly used Eg peak width, are both effective metrics for evaluating the quality of PtSe2: films with narrower Eg and A1g peaks exhibit higher in-plane and out-of-plane crystalline quality, as well as higher sheet conductance. Finally, coplanar waveguides integrating a semimetallic PtSe2 channel are fabricated on a 2-inch sapphire substrate to demonstrate optoelectronic devices operating at the 1.55 um telecom wavelength. This includes photodetectors with a record bandwidth of 60 GHz and the first PtSe2-based optoelectronic mixer with a 30 GHz bandwidth.
title Growth of Highly Conductive PtSe2 Films Controlled by Raman Metrics for High-Frequency Photodetectors and Optoelectronic Mixers at 1.55 μm
topic Materials Science
Applied Physics
url https://arxiv.org/abs/2503.20659