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Autores principales: Kirya, Paula, Hochberg, Justin D., Kim, Han Sol, Haddadin, Zaid, Bordy, Samantha, Byun, Jiuk, Pokorski, Jonathan K., Poulikakos, Lisa V.
Formato: Preprint
Publicado: 2025
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Acceso en línea:https://arxiv.org/abs/2504.11657
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author Kirya, Paula
Hochberg, Justin D.
Kim, Han Sol
Haddadin, Zaid
Bordy, Samantha
Byun, Jiuk
Pokorski, Jonathan K.
Poulikakos, Lisa V.
author_facet Kirya, Paula
Hochberg, Justin D.
Kim, Han Sol
Haddadin, Zaid
Bordy, Samantha
Byun, Jiuk
Pokorski, Jonathan K.
Poulikakos, Lisa V.
contents Metasurfaces have pioneered significant improvements in sensing technology by tailoring strong optical responses to weak signals. When designed with anisotropic subwavelength geometries, metasurfaces can tune responses to varying polarization states of light. Leveraging this to quantify structural alignment in fibrous materials unveils an alternative to destructive characterization methods. This work introduces metasurface-enhanced polarized light microscopy (Meta-PoL), which employs polarization-tunable, guided-mode-resonant colorimetric metasurfaces to characterize molecular and bulk alignment of poly(ε-caprolactone) (PCL) nanofibers in a far-field configuration. PCL nanofibers drawn at 0%, 400%, and 900% ratios were interfaced with the studied metasurfaces. Metasurface resonances coinciding with the intrinsic drawn nanofiber resonances - confirmed by Stokes Polarimetry - produced the strongest colorimetric enhancement, resultant from alignment-specific nanofiber reflectivity. The enhancement degree corresponded with molecular and bulk alignments for each draw ratio, as measured through differential scanning calorimetry and scanning electron microscopy, respectively. Thus, Meta-PoL presents an all-optical, non-destructive, and quantitative measurement of nanofiber alignment.
format Preprint
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institution arXiv
publishDate 2025
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spellingShingle Polarization-Tunable Colorimetric Metasurfaces for All-Optical and Non-Destructive Structural Characterization of Polymeric Nanofibers
Kirya, Paula
Hochberg, Justin D.
Kim, Han Sol
Haddadin, Zaid
Bordy, Samantha
Byun, Jiuk
Pokorski, Jonathan K.
Poulikakos, Lisa V.
Optics
Metasurfaces have pioneered significant improvements in sensing technology by tailoring strong optical responses to weak signals. When designed with anisotropic subwavelength geometries, metasurfaces can tune responses to varying polarization states of light. Leveraging this to quantify structural alignment in fibrous materials unveils an alternative to destructive characterization methods. This work introduces metasurface-enhanced polarized light microscopy (Meta-PoL), which employs polarization-tunable, guided-mode-resonant colorimetric metasurfaces to characterize molecular and bulk alignment of poly(ε-caprolactone) (PCL) nanofibers in a far-field configuration. PCL nanofibers drawn at 0%, 400%, and 900% ratios were interfaced with the studied metasurfaces. Metasurface resonances coinciding with the intrinsic drawn nanofiber resonances - confirmed by Stokes Polarimetry - produced the strongest colorimetric enhancement, resultant from alignment-specific nanofiber reflectivity. The enhancement degree corresponded with molecular and bulk alignments for each draw ratio, as measured through differential scanning calorimetry and scanning electron microscopy, respectively. Thus, Meta-PoL presents an all-optical, non-destructive, and quantitative measurement of nanofiber alignment.
title Polarization-Tunable Colorimetric Metasurfaces for All-Optical and Non-Destructive Structural Characterization of Polymeric Nanofibers
topic Optics
url https://arxiv.org/abs/2504.11657