Laser, Vacuum, and Gas Reaction Chamber for Operando Measurements at NSLS-II's 28-ID-2
Fuente:
arXiv
Saved in:
| Main Authors: | , , , , , , , , , , , , , |
|---|---|
| Format: | Preprint |
| Published: |
2025
|
| Subjects: | |
| Online Access: | |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| _version_ | 1866918280164278272 |
|---|---|
| author | Moghimi, Lauren Y. Johansson, Patrik Paul, Subhechchha Wang, Yifan Irvine, Sara Graham, Remington Taylor, Zane Martinez, Angel A. Markert, John T. Trunk, John Zhong, Hui Bai, Jianming Ghose, Sanjit Dresselhaus-Marais, Leora |
| author_facet | Moghimi, Lauren Y. Johansson, Patrik Paul, Subhechchha Wang, Yifan Irvine, Sara Graham, Remington Taylor, Zane Martinez, Angel A. Markert, John T. Trunk, John Zhong, Hui Bai, Jianming Ghose, Sanjit Dresselhaus-Marais, Leora |
| contents | We present a laser reaction chamber that we developed for in-situ/operando X-ray diffraction measurements at the NSLS-II 28-ID-2 XPD (X-Ray Powder Diffraction) beamline. This chamber allows for rapid and dynamic sample heating under specialized gas environments, spanning ambient conditions down to vacuum pressures. We demonstrate the capabilities of this setup through two applications: laser-driven heating in polycrystalline iron oxide and in single crystal WTe2. Our measurements reveal the ability to resolve chemical reaction kinetics over minutes with 1-s time resolution. This setup advances opportunities for in-situ/operando XRD studies in both bulk and single crystal materials. |
| format | Preprint |
| id |
arxiv_https___arxiv_org_abs_2505_10720 |
| institution | arXiv |
| publishDate | 2025 |
| record_format | arxiv |
| spellingShingle | Laser, Vacuum, and Gas Reaction Chamber for Operando Measurements at NSLS-II's 28-ID-2 Moghimi, Lauren Y. Johansson, Patrik Paul, Subhechchha Wang, Yifan Irvine, Sara Graham, Remington Taylor, Zane Martinez, Angel A. Markert, John T. Trunk, John Zhong, Hui Bai, Jianming Ghose, Sanjit Dresselhaus-Marais, Leora Instrumentation and Detectors Materials Science We present a laser reaction chamber that we developed for in-situ/operando X-ray diffraction measurements at the NSLS-II 28-ID-2 XPD (X-Ray Powder Diffraction) beamline. This chamber allows for rapid and dynamic sample heating under specialized gas environments, spanning ambient conditions down to vacuum pressures. We demonstrate the capabilities of this setup through two applications: laser-driven heating in polycrystalline iron oxide and in single crystal WTe2. Our measurements reveal the ability to resolve chemical reaction kinetics over minutes with 1-s time resolution. This setup advances opportunities for in-situ/operando XRD studies in both bulk and single crystal materials. |
| title | Laser, Vacuum, and Gas Reaction Chamber for Operando Measurements at NSLS-II's 28-ID-2 |
| topic | Instrumentation and Detectors Materials Science |
| url | https://arxiv.org/abs/2505.10720 |