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| Main Authors: | , , , |
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| Format: | Preprint |
| Published: |
2025
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| Subjects: | |
| Online Access: | https://arxiv.org/abs/2506.04543 |
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| _version_ | 1866916780722618368 |
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| author | Hultquist, Riley J. Simonne, David Mondal, Sayantan Jossou, Ericmoore |
| author_facet | Hultquist, Riley J. Simonne, David Mondal, Sayantan Jossou, Ericmoore |
| contents | We present the design of a modular multipurpose cell for monitoring the degradation of materials in extreme environments. This cell decouples the reference electrode from the working and counter electrodes, permitting precise electrochemical control and measurement reliability. The design is compatible with 4th generation synchrotron light sources, and its emphasis on modularity facilitates adaptation to different beamlines, where there may be variations in sample stage requirements and X-ray imaging techniques. Experimental tests with the novel design demonstrate its support of real-time corrosion and hydrogen embrittlement measurements under both Bragg Coherent Diffraction Imaging (BCDI) and Dark Field X-ray Microscopy (DFXM) configurations. |
| format | Preprint |
| id |
arxiv_https___arxiv_org_abs_2506_04543 |
| institution | arXiv |
| publishDate | 2025 |
| record_format | arxiv |
| spellingShingle | Multipurpose in situ cell design for 3D X-ray imaging of electrochemical processes Hultquist, Riley J. Simonne, David Mondal, Sayantan Jossou, Ericmoore Instrumentation and Detectors Materials Science We present the design of a modular multipurpose cell for monitoring the degradation of materials in extreme environments. This cell decouples the reference electrode from the working and counter electrodes, permitting precise electrochemical control and measurement reliability. The design is compatible with 4th generation synchrotron light sources, and its emphasis on modularity facilitates adaptation to different beamlines, where there may be variations in sample stage requirements and X-ray imaging techniques. Experimental tests with the novel design demonstrate its support of real-time corrosion and hydrogen embrittlement measurements under both Bragg Coherent Diffraction Imaging (BCDI) and Dark Field X-ray Microscopy (DFXM) configurations. |
| title | Multipurpose in situ cell design for 3D X-ray imaging of electrochemical processes |
| topic | Instrumentation and Detectors Materials Science |
| url | https://arxiv.org/abs/2506.04543 |