In situ growth of a type-II ZnO/ZnS heterostructure:From stability to band-offset

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Main Authors: de Oliveira, P. R. A, Coelho, I., Felix, G., Venezuela, P., Stavale, F.
Format: Preprint
Published: 2025
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author de Oliveira, P. R. A
Coelho, I.
Felix, G.
Venezuela, P.
Stavale, F.
author_facet de Oliveira, P. R. A
Coelho, I.
Felix, G.
Venezuela, P.
Stavale, F.
contents We have successfully obtained a ZnO/ZnS heterostructure by heating a ZnS(001) single crystal in a controlled impurities-free oxygen atmosphere. Combining X-ray photoelectron spectroscopy (XPS), and atomic force microscopy (AFM), we explore the stability, electronic structure, and morphology of that interface. Our XPS measurements reveal a binding energy shift of the core-level peaks, indicating a band-bending effect due to the formation of a hybrid ZnO/ZnS interface. In addition, AFM measurements show that exposure of ZnS single-crystal to an oxygen atmosphere leads to the formation of ZnO/ZnS-like islands. Interestingly, our band-offset estimation suggest a type-II heterostructure arrangement with suitable electronic edges positions that turn ZnO/ZnS heterostructure a promising platform for catalytic applications, particularly hydrogen and oxygen evolution reactions.
format Preprint
id arxiv_https___arxiv_org_abs_2506_14499
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle In situ growth of a type-II ZnO/ZnS heterostructure:From stability to band-offset
de Oliveira, P. R. A
Coelho, I.
Felix, G.
Venezuela, P.
Stavale, F.
Materials Science
We have successfully obtained a ZnO/ZnS heterostructure by heating a ZnS(001) single crystal in a controlled impurities-free oxygen atmosphere. Combining X-ray photoelectron spectroscopy (XPS), and atomic force microscopy (AFM), we explore the stability, electronic structure, and morphology of that interface. Our XPS measurements reveal a binding energy shift of the core-level peaks, indicating a band-bending effect due to the formation of a hybrid ZnO/ZnS interface. In addition, AFM measurements show that exposure of ZnS single-crystal to an oxygen atmosphere leads to the formation of ZnO/ZnS-like islands. Interestingly, our band-offset estimation suggest a type-II heterostructure arrangement with suitable electronic edges positions that turn ZnO/ZnS heterostructure a promising platform for catalytic applications, particularly hydrogen and oxygen evolution reactions.
title In situ growth of a type-II ZnO/ZnS heterostructure:From stability to band-offset
topic Materials Science
url https://arxiv.org/abs/2506.14499