Quantitative structure determination from experimental four-dimensional scanning transmission electron microscopy via the scattering matrix

Fuente: arXiv
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Autori principali: Terzoudis-Lumsden, Emmanuel W. C., Sadri, Alireza, Weyland, Matthew, Bourgeois, Laure, Ribet, Stephanie M., Varnavides, Georgios, Ophus, Colin, Petersen, Timothy C., Findlay, Scott D.
Natura: Preprint
Pubblicazione: 2025
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author Terzoudis-Lumsden, Emmanuel W. C.
Sadri, Alireza
Weyland, Matthew
Bourgeois, Laure
Ribet, Stephanie M.
Varnavides, Georgios
Ophus, Colin
Petersen, Timothy C.
Findlay, Scott D.
author_facet Terzoudis-Lumsden, Emmanuel W. C.
Sadri, Alireza
Weyland, Matthew
Bourgeois, Laure
Ribet, Stephanie M.
Varnavides, Georgios
Ophus, Colin
Petersen, Timothy C.
Findlay, Scott D.
contents Considerable inroads have recently been made on algorithms to determine the sample potential from four-dimensional scanning transmission electron microscopy data from thick samples where multiple scattering cannot be neglected. This paper further develops the scattering matrix approach to such structure determination. Through simulation, we demonstrate how this approach can be modified to better handle partial spatial coherence, unknown probe defocus, and information from the dark field region. By combining these developments we reconstruct the electrostatic potential of a monolithic SrTiO$_3$ crystal showing good quantitative agreement with the expected structure.
format Preprint
id arxiv_https___arxiv_org_abs_2506_21004
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Quantitative structure determination from experimental four-dimensional scanning transmission electron microscopy via the scattering matrix
Terzoudis-Lumsden, Emmanuel W. C.
Sadri, Alireza
Weyland, Matthew
Bourgeois, Laure
Ribet, Stephanie M.
Varnavides, Georgios
Ophus, Colin
Petersen, Timothy C.
Findlay, Scott D.
Materials Science
Instrumentation and Detectors
Considerable inroads have recently been made on algorithms to determine the sample potential from four-dimensional scanning transmission electron microscopy data from thick samples where multiple scattering cannot be neglected. This paper further develops the scattering matrix approach to such structure determination. Through simulation, we demonstrate how this approach can be modified to better handle partial spatial coherence, unknown probe defocus, and information from the dark field region. By combining these developments we reconstruct the electrostatic potential of a monolithic SrTiO$_3$ crystal showing good quantitative agreement with the expected structure.
title Quantitative structure determination from experimental four-dimensional scanning transmission electron microscopy via the scattering matrix
topic Materials Science
Instrumentation and Detectors
url https://arxiv.org/abs/2506.21004