Colossal Effect of Nanopore Surface Ionic Charge on the Dynamics of Confined Water

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Hauptverfasser: Mozhdehei, Armin, Lenz, Philip, Gries, Stella, Meinert, Sophia-Marie, Lefort, Ronan, Zanotti, Jean-Marc, Berrod, Quentin, Appel, Markus, Busch, Mark, Huber, Patrick, Fröba, Michael, Morineau, Denis
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Veröffentlicht: 2025
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author Mozhdehei, Armin
Lenz, Philip
Gries, Stella
Meinert, Sophia-Marie
Lefort, Ronan
Zanotti, Jean-Marc
Berrod, Quentin
Appel, Markus
Busch, Mark
Huber, Patrick
Fröba, Michael
Morineau, Denis
author_facet Mozhdehei, Armin
Lenz, Philip
Gries, Stella
Meinert, Sophia-Marie
Lefort, Ronan
Zanotti, Jean-Marc
Berrod, Quentin
Appel, Markus
Busch, Mark
Huber, Patrick
Fröba, Michael
Morineau, Denis
contents Interfacial interactions significantly alter the fundamental properties of water confined in mesoporous structures, with crucial implications for geological, physicochemical, and biological processes. Herein, we focused on the effect of changing the surface ionic charge of nanopores with comparable pore size (3.5-3.8 nm) on the dynamics of confined liquid water. The control of the pore surface ionicity was achieved by using two periodic mesoporous organosilicas (PMOs) containing either neutral or charged forms of a chemically similar bridging unit. The effect on the dynamics of water at the nanoscale was investigated in the temperature range of 245 -300 K, encompassing the glass transition by incoherent quasielastic neutron scattering (QENS), For both types of PMOs, the water dynamics revealed two distinct types of molecular motions: rapid local movements and translational jump diffusion. While the neutral PMO induces a moderate confinement effect, we show that the charged PMO drastically slows down water dynamics, reducing translational diffusion by a factor of four and increasing residence time by an order of magnitude. Notably, by changing the pore filling values, we demonstrate that for charged pore this effect extends beyond the interfacial layer of surface-bound water molecules to encompass the entire pore volume. Thus, our observation indicates a dramatic change in the long-range character of the interaction of water confined in nanopores with surface ionic charge compared to a simple change in hydrophilicity. This is relevant for the understanding of a broad variety of applications in (nano)technological phenomena and processes, such as nanofiltration and membrane design.
format Preprint
id arxiv_https___arxiv_org_abs_2509_19802
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Colossal Effect of Nanopore Surface Ionic Charge on the Dynamics of Confined Water
Mozhdehei, Armin
Lenz, Philip
Gries, Stella
Meinert, Sophia-Marie
Lefort, Ronan
Zanotti, Jean-Marc
Berrod, Quentin
Appel, Markus
Busch, Mark
Huber, Patrick
Fröba, Michael
Morineau, Denis
Chemical Physics
Interfacial interactions significantly alter the fundamental properties of water confined in mesoporous structures, with crucial implications for geological, physicochemical, and biological processes. Herein, we focused on the effect of changing the surface ionic charge of nanopores with comparable pore size (3.5-3.8 nm) on the dynamics of confined liquid water. The control of the pore surface ionicity was achieved by using two periodic mesoporous organosilicas (PMOs) containing either neutral or charged forms of a chemically similar bridging unit. The effect on the dynamics of water at the nanoscale was investigated in the temperature range of 245 -300 K, encompassing the glass transition by incoherent quasielastic neutron scattering (QENS), For both types of PMOs, the water dynamics revealed two distinct types of molecular motions: rapid local movements and translational jump diffusion. While the neutral PMO induces a moderate confinement effect, we show that the charged PMO drastically slows down water dynamics, reducing translational diffusion by a factor of four and increasing residence time by an order of magnitude. Notably, by changing the pore filling values, we demonstrate that for charged pore this effect extends beyond the interfacial layer of surface-bound water molecules to encompass the entire pore volume. Thus, our observation indicates a dramatic change in the long-range character of the interaction of water confined in nanopores with surface ionic charge compared to a simple change in hydrophilicity. This is relevant for the understanding of a broad variety of applications in (nano)technological phenomena and processes, such as nanofiltration and membrane design.
title Colossal Effect of Nanopore Surface Ionic Charge on the Dynamics of Confined Water
topic Chemical Physics
url https://arxiv.org/abs/2509.19802