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Autori principali: Shiryaev, A. A., Zhukov, A. N., Yakushev, V. V., Averin, A. A., Yapaskurt, V. O., Borisova, A. Yu., Bychkov, A. Yu., Safonov, O. G., Lomonosov, I. V.
Natura: Preprint
Pubblicazione: 2025
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Accesso online:https://arxiv.org/abs/2509.23446
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Sommario:
  • Large single crystals of natural zircon were shock-loaded at 13.6 and 51.3 GPa in planar geometry. No structural changes were observed after loading at 13.6 GPa. Loading to 51.3 GPa resulted in zircon transformation to a denser scheelite-structured phase, reidite. The investigation of reidite samples by X-ray diffraction, Raman, photo- and cathodoluminescence spectroscopies revealed segregation of some trace cations (such as REE) on planar defects during the transformation. The segregation has occurred in a laboratory experiment without long-term annealing after the shock loading. A possible mechanism of the segregation of trivalent trace cations assumes local violation of charge balance during the zircon-reidite reconstructive transformation, which is accompanied by changes in the topology of polyhedra and second coordination spheres (Si-Zr). This results in expulsion of a fraction of the trace elements into energetically expensive interstitial positions with high diffusivity even at relatively low temperatures.