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Bibliographic Details
Main Authors: Lee, Yeri, Oh, Juseung, Ma, Kyung Yeol, Lee, Seung Jin, Jung, Eui Young, Wang, Yani, Watanabe, Kenji, Taniguchi, Takashi, Peng, Hailin, Ago, Hiroki, Kim, Ki Kang, Shin, Hyeon Suk, Ryu, Sunmin
Format: Preprint
Published: 2025
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Online Access:https://arxiv.org/abs/2509.25910
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Table of Contents:
  • Hexagonal boron nitride (hBN) supports a wide range of two-dimensional (2D) technologies, yet assessing its crystalline quality over large areas remains a fundamental challenge. Both antiparallel domains, an intrinsic outcome of epitaxy on high-symmetry substrates, and associated structural defects have long evaded optical detection. Here, we show that interferometric second-harmonic generation (SHG) imaging provides a powerful, nondestructive probe of lattice orientation and structural integrity in chemical vapor deposition-grown hBN. This approach reveals the ubiquitous formation of antiparallel domains and quantifies their impact on crystalline order. SHG intensity also emerges as a direct optical metric of domain disorder, spanning three orders of magnitude across films produced by ten different growth routes. Correlation with Raman spectroscopy establishes a unified framework for evaluating crystalline quality. Beyond hBN, this method offers a high-throughput route to wide-area structural imaging in various non-centrosymmetric materials, advancing their deployment in electronics, photonics, and quantum technologies.