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Autores principales: Anwar, Tarique, DallAglio, Diana, Sabzehparvar, Milad, Tagliabue, Giulia
Formato: Preprint
Publicado: 2025
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Acceso en línea:https://arxiv.org/abs/2510.08809
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author Anwar, Tarique
DallAglio, Diana
Sabzehparvar, Milad
Tagliabue, Giulia
author_facet Anwar, Tarique
DallAglio, Diana
Sabzehparvar, Milad
Tagliabue, Giulia
contents Light and heat drive interfacial chemistry at solid-liquid interfaces, underpinning processes central to sustainable energy conversion, including photoelectrochemical and hydrovoltaic systems. Yet, non-invasive probing of light-induced interfacial dynamics remains challenging due to the weak and spatially complex nature of optical signals. Here, we introduce a nanophotonic platform that enhances second harmonic generation (SHG) from nanostructured interfaces by over two orders of magnitude, enabling real-time, all-optical access to interfacial processes. We develop a rigorous overlap-integral formalism that provides a general quantitative framework for SHG in nanostructured geometries. By accounting for spatially inhomogeneous electromagnetic fields, this approach links the nonlinear response to geometry-dependent near-field and reveals new degrees of freedom, namely independent control of attenuation and phase, which are absent in planar systems. This enables deterministic tuning of surface and electric-field-induced contributions through nanophotonic design. Using in situ SHG at silicon-oxide-electrolyte interfaces, we resolve subtle spectral shifts of ~1.3 nm with electrolyte concentration, indicating coupling between electrical double layer potential and semiconductor polarizability. Under controlled optical excitation, we observe reversible, intensity-dependent modulation of interfacial susceptibility, with a decrease at low intensities consistent with photocharging and an increase at higher intensities due to photothermal effects. These results establish nanophotonic-enhanced SHG as a quantitative and tunable probe of interfacial phenomena, providing a unified framework linking optical response, electrostatics, and geometry, and opening new avenues for controlling interfacial charge and potential with light for applications in energy conversion, catalysis, and nanophotonic devices.
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spellingShingle Revealing Light-Driven Dynamics at Nanostructured Solid-Liquid Interfaces with In-Situ SHG
Anwar, Tarique
DallAglio, Diana
Sabzehparvar, Milad
Tagliabue, Giulia
Chemical Physics
Light and heat drive interfacial chemistry at solid-liquid interfaces, underpinning processes central to sustainable energy conversion, including photoelectrochemical and hydrovoltaic systems. Yet, non-invasive probing of light-induced interfacial dynamics remains challenging due to the weak and spatially complex nature of optical signals. Here, we introduce a nanophotonic platform that enhances second harmonic generation (SHG) from nanostructured interfaces by over two orders of magnitude, enabling real-time, all-optical access to interfacial processes. We develop a rigorous overlap-integral formalism that provides a general quantitative framework for SHG in nanostructured geometries. By accounting for spatially inhomogeneous electromagnetic fields, this approach links the nonlinear response to geometry-dependent near-field and reveals new degrees of freedom, namely independent control of attenuation and phase, which are absent in planar systems. This enables deterministic tuning of surface and electric-field-induced contributions through nanophotonic design. Using in situ SHG at silicon-oxide-electrolyte interfaces, we resolve subtle spectral shifts of ~1.3 nm with electrolyte concentration, indicating coupling between electrical double layer potential and semiconductor polarizability. Under controlled optical excitation, we observe reversible, intensity-dependent modulation of interfacial susceptibility, with a decrease at low intensities consistent with photocharging and an increase at higher intensities due to photothermal effects. These results establish nanophotonic-enhanced SHG as a quantitative and tunable probe of interfacial phenomena, providing a unified framework linking optical response, electrostatics, and geometry, and opening new avenues for controlling interfacial charge and potential with light for applications in energy conversion, catalysis, and nanophotonic devices.
title Revealing Light-Driven Dynamics at Nanostructured Solid-Liquid Interfaces with In-Situ SHG
topic Chemical Physics
url https://arxiv.org/abs/2510.08809