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Main Authors: Lazareno, Katelyn, Chae, Christopher, Haight, Becky, Jabin, Shams, Steinhardt, Rachel, Plombon, John J., Rajan, Siddharth, Woodward, Patrick M., Hwang, Jinwoo, Yang, Fengyuan
Format: Preprint
Published: 2025
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Online Access:https://arxiv.org/abs/2510.17672
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author Lazareno, Katelyn
Chae, Christopher
Haight, Becky
Jabin, Shams
Steinhardt, Rachel
Plombon, John J.
Rajan, Siddharth
Woodward, Patrick M.
Hwang, Jinwoo
Yang, Fengyuan
author_facet Lazareno, Katelyn
Chae, Christopher
Haight, Becky
Jabin, Shams
Steinhardt, Rachel
Plombon, John J.
Rajan, Siddharth
Woodward, Patrick M.
Hwang, Jinwoo
Yang, Fengyuan
contents To investigate the scope of ferroelectric behavior in La-substituted BiFeO3 films, LaxBi1-xFeO3 epitaxial films were synthesized using off-axis co-sputtering on SrTiO3(001) and DyScO3(110) substrates with a SrRuO3 bottom electrode layer. A digital-doping deposition method was used to enable precise control and continuous tuning of La concentration in high-quality LaxBi1-xFeO3 films across a wide range of x = 0.05-0.60, which was systematically investigated using piezoresponse force microscopy. Robust and reversible out-of-plane ferroelectric switching has been observed up to x = 0.35, while films with x $\geq$ 0.37 exhibit no measurable ferroelectric behavior, indicating a sharp ferroelectric-to-paraelectric phase transition between x = 0.35 and 0.37. This represents the highest reported La concentration in LaxBi1-xFeO3 films that retains ferroelectric ordering, highlighting opportunities to engineer ferroelectric and multiferroic properties in complex oxide heterostructures.
format Preprint
id arxiv_https___arxiv_org_abs_2510_17672
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Broad-Range Tuning of Ferroelectric Switching of LaxBi1-xFeO3 Epitaxial Films via Digital Doping using Off-Axis Co-Sputtering
Lazareno, Katelyn
Chae, Christopher
Haight, Becky
Jabin, Shams
Steinhardt, Rachel
Plombon, John J.
Rajan, Siddharth
Woodward, Patrick M.
Hwang, Jinwoo
Yang, Fengyuan
Materials Science
To investigate the scope of ferroelectric behavior in La-substituted BiFeO3 films, LaxBi1-xFeO3 epitaxial films were synthesized using off-axis co-sputtering on SrTiO3(001) and DyScO3(110) substrates with a SrRuO3 bottom electrode layer. A digital-doping deposition method was used to enable precise control and continuous tuning of La concentration in high-quality LaxBi1-xFeO3 films across a wide range of x = 0.05-0.60, which was systematically investigated using piezoresponse force microscopy. Robust and reversible out-of-plane ferroelectric switching has been observed up to x = 0.35, while films with x $\geq$ 0.37 exhibit no measurable ferroelectric behavior, indicating a sharp ferroelectric-to-paraelectric phase transition between x = 0.35 and 0.37. This represents the highest reported La concentration in LaxBi1-xFeO3 films that retains ferroelectric ordering, highlighting opportunities to engineer ferroelectric and multiferroic properties in complex oxide heterostructures.
title Broad-Range Tuning of Ferroelectric Switching of LaxBi1-xFeO3 Epitaxial Films via Digital Doping using Off-Axis Co-Sputtering
topic Materials Science
url https://arxiv.org/abs/2510.17672