Density and excess molar enthalpy of (2-propanol + glyme) liquid mixtures. Application of the Flory model

Fuente: arXiv
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Main Authors: Alves-Laurentino, João Victor, Pazoki, Fatemeh, Sanz, Luis Felipe, González, Juan Antonio, Hevia, Fernando, Lozano-Martín, Daniel
Format: Preprint
Published: 2025
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author Alves-Laurentino, João Victor
Pazoki, Fatemeh
Sanz, Luis Felipe
González, Juan Antonio
Hevia, Fernando
Lozano-Martín, Daniel
author_facet Alves-Laurentino, João Victor
Pazoki, Fatemeh
Sanz, Luis Felipe
González, Juan Antonio
Hevia, Fernando
Lozano-Martín, Daniel
contents For glymes of general formula CH3O(CH2CH2O)uCH3, with u = 1, 2, 3, 4, the densities of the (2-propanol + glyme) systems at temperatures ranging from (293.15 to 303.15) K and at pressure 0.1 MPa were determined using a DSA 5000 densimeter (from Anton Paar). The corresponding excess molar volumes were calculated from these density measurements. In addition, excess molar enthalpies at 298.15 K and 0.1 MPa were measured using a Tian-Calvet micro-calorimeter. The results show that alkanol-ether interactions are strong but do not contribute significantly to the excess molar enthalpy, as the values are large and positive, and comparable to those of (glyme + n-heptane) systems. The excess molar volumes are small or even negative (in the case of the mixture with u = 4), indicating that they are mainly governed by structural effects. Mixtures with 1-propanol or 2-propanol behave similarly, although interactions between unlike molecules become slightly stronger when 1-propanol is involved. On the other hand, effects related to alcohol self-association play a decisive role in the thermodynamic properties when glymes are replaced by di-n-propyl ether. This is supported by the application of the Flory model, which shows that orientational effects are weak in the studied glyme-containing mixtures but become significantly stronger when di-n-propyl ether is considered.
format Preprint
id arxiv_https___arxiv_org_abs_2511_17057
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Density and excess molar enthalpy of (2-propanol + glyme) liquid mixtures. Application of the Flory model
Alves-Laurentino, João Victor
Pazoki, Fatemeh
Sanz, Luis Felipe
González, Juan Antonio
Hevia, Fernando
Lozano-Martín, Daniel
Chemical Physics
For glymes of general formula CH3O(CH2CH2O)uCH3, with u = 1, 2, 3, 4, the densities of the (2-propanol + glyme) systems at temperatures ranging from (293.15 to 303.15) K and at pressure 0.1 MPa were determined using a DSA 5000 densimeter (from Anton Paar). The corresponding excess molar volumes were calculated from these density measurements. In addition, excess molar enthalpies at 298.15 K and 0.1 MPa were measured using a Tian-Calvet micro-calorimeter. The results show that alkanol-ether interactions are strong but do not contribute significantly to the excess molar enthalpy, as the values are large and positive, and comparable to those of (glyme + n-heptane) systems. The excess molar volumes are small or even negative (in the case of the mixture with u = 4), indicating that they are mainly governed by structural effects. Mixtures with 1-propanol or 2-propanol behave similarly, although interactions between unlike molecules become slightly stronger when 1-propanol is involved. On the other hand, effects related to alcohol self-association play a decisive role in the thermodynamic properties when glymes are replaced by di-n-propyl ether. This is supported by the application of the Flory model, which shows that orientational effects are weak in the studied glyme-containing mixtures but become significantly stronger when di-n-propyl ether is considered.
title Density and excess molar enthalpy of (2-propanol + glyme) liquid mixtures. Application of the Flory model
topic Chemical Physics
url https://arxiv.org/abs/2511.17057