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Main Authors: Primer, Micaela E., Berseneva, Anna A., Ulde, Ayesha, Sun, Wenhao, Smaha, Rebecca W.
Format: Preprint
Published: 2025
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Online Access:https://arxiv.org/abs/2512.00253
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author Primer, Micaela E.
Berseneva, Anna A.
Ulde, Ayesha
Sun, Wenhao
Smaha, Rebecca W.
author_facet Primer, Micaela E.
Berseneva, Anna A.
Ulde, Ayesha
Sun, Wenhao
Smaha, Rebecca W.
contents Subtle synthetic variables can have an outsizes influence on the crystal structure and magnetic properties of a material, particularly those of quantum materials. In this work, we investigate the impact of synthesis under a magnetic field (magnetosynthesis) on the crystal structure and magnetic properties of several Cu$^{2+}$ ($S=1/2$) based materials with antiferromagnetic interactions and varying levels of magnetic frustration, from simple antiferromagnets to a quantum spin liquid. We employ small (0.09 - 0.37 T) magnetic fields applied during low-temperature hydrothermal or evaporative synthesis of the simple antiferromagnet CuCl$_2\cdot$2H$_2$O, the canted antiferromagnet (Cu,Zn)$_3$Cl$_4$(OH)$_2\cdot$2H$_2$O, the frustrated and canted antiferromagnet atacamite Cu$_2$(OH)$_3$Cl, and the highly frustrated quantum spin liquid herbertsmithite Cu$_3$Zn(OH)$_6$Cl$_2$. We found that (Cu,Zn)$_3$Cl$_4$(OH)$_2\cdot$2H$_2$O experiences structural changes well above its magnetic transition. Atacamite Cu$_2$(OH)$_3$Cl synthesized under a 0.19 T field experiences a 0.15 K (~3%) decrease in its Néel transition temperature and a significant strengthening of its antiferromagnetic interactions, suggesting that magnetosynthesis can influence the ground state of moderately frustrated materials.
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publishDate 2025
record_format arxiv
spellingShingle Magnetosynthesis effect on the structure and ground state of Cu$^{2+}$-based antiferromagnets
Primer, Micaela E.
Berseneva, Anna A.
Ulde, Ayesha
Sun, Wenhao
Smaha, Rebecca W.
Strongly Correlated Electrons
Materials Science
Subtle synthetic variables can have an outsizes influence on the crystal structure and magnetic properties of a material, particularly those of quantum materials. In this work, we investigate the impact of synthesis under a magnetic field (magnetosynthesis) on the crystal structure and magnetic properties of several Cu$^{2+}$ ($S=1/2$) based materials with antiferromagnetic interactions and varying levels of magnetic frustration, from simple antiferromagnets to a quantum spin liquid. We employ small (0.09 - 0.37 T) magnetic fields applied during low-temperature hydrothermal or evaporative synthesis of the simple antiferromagnet CuCl$_2\cdot$2H$_2$O, the canted antiferromagnet (Cu,Zn)$_3$Cl$_4$(OH)$_2\cdot$2H$_2$O, the frustrated and canted antiferromagnet atacamite Cu$_2$(OH)$_3$Cl, and the highly frustrated quantum spin liquid herbertsmithite Cu$_3$Zn(OH)$_6$Cl$_2$. We found that (Cu,Zn)$_3$Cl$_4$(OH)$_2\cdot$2H$_2$O experiences structural changes well above its magnetic transition. Atacamite Cu$_2$(OH)$_3$Cl synthesized under a 0.19 T field experiences a 0.15 K (~3%) decrease in its Néel transition temperature and a significant strengthening of its antiferromagnetic interactions, suggesting that magnetosynthesis can influence the ground state of moderately frustrated materials.
title Magnetosynthesis effect on the structure and ground state of Cu$^{2+}$-based antiferromagnets
topic Strongly Correlated Electrons
Materials Science
url https://arxiv.org/abs/2512.00253