Optical refractive index measurements of AlGaAs at high temperature for fully automated molecular beam epitaxy growth of Bragg mirrors

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Main Authors: Gadras, Pierre, Bourdon, Léo, Fées, Antoine, Saddik, Karim Ben, Almuneau, Guilhem, Arnoult, Alexandre
Format: Preprint
Published: 2025
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author Gadras, Pierre
Bourdon, Léo
Fées, Antoine
Saddik, Karim Ben
Almuneau, Guilhem
Arnoult, Alexandre
author_facet Gadras, Pierre
Bourdon, Léo
Fées, Antoine
Saddik, Karim Ben
Almuneau, Guilhem
Arnoult, Alexandre
contents In-situ measurement is a key feature to better understand and precisely control the growth of complex structures, such as vertical-cavity surface-emitting lasers. In this work, we are showing the precise measurement of optical indices of AlGaAs at 600 {\textdegree}C over a wide spectral range (450--1400 nm). To do so, in-situ spectral reflectance measurement is used, combined with ex-situ layer thickness and composition measurement by x-ray diffraction enabling for precise determination of the optical indices with an accuracy better than 1%. To validate our measurements, we realized the complete automation of the growth of a GaAs/AlAs 940 nm-DBR by molecular beam epitaxy, without the need to pre-calibrate cells fluxes. The fabricated DBR shows a deviation of 0.2 nm of the stop-band central-wavelength compared to the targeted one. This approach holds significant interest for the III--V semiconductor community and epitaxial growth techniques.
format Preprint
id arxiv_https___arxiv_org_abs_2512_01472
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Optical refractive index measurements of AlGaAs at high temperature for fully automated molecular beam epitaxy growth of Bragg mirrors
Gadras, Pierre
Bourdon, Léo
Fées, Antoine
Saddik, Karim Ben
Almuneau, Guilhem
Arnoult, Alexandre
Materials Science
In-situ measurement is a key feature to better understand and precisely control the growth of complex structures, such as vertical-cavity surface-emitting lasers. In this work, we are showing the precise measurement of optical indices of AlGaAs at 600 {\textdegree}C over a wide spectral range (450--1400 nm). To do so, in-situ spectral reflectance measurement is used, combined with ex-situ layer thickness and composition measurement by x-ray diffraction enabling for precise determination of the optical indices with an accuracy better than 1%. To validate our measurements, we realized the complete automation of the growth of a GaAs/AlAs 940 nm-DBR by molecular beam epitaxy, without the need to pre-calibrate cells fluxes. The fabricated DBR shows a deviation of 0.2 nm of the stop-band central-wavelength compared to the targeted one. This approach holds significant interest for the III--V semiconductor community and epitaxial growth techniques.
title Optical refractive index measurements of AlGaAs at high temperature for fully automated molecular beam epitaxy growth of Bragg mirrors
topic Materials Science
url https://arxiv.org/abs/2512.01472