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Main Authors: Nakashima, Philip N. H., Shao, Yu-Tsun, Zhang, Zezhong, Smith, Andrew E., Liu, Tianyu, Medhekar, Nikhil V., Etheridge, Joanne, Bourgeois, Laure, Zuo, Jian-Min
Format: Preprint
Published: 2025
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Online Access:https://arxiv.org/abs/2512.05296
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author Nakashima, Philip N. H.
Shao, Yu-Tsun
Zhang, Zezhong
Smith, Andrew E.
Liu, Tianyu
Medhekar, Nikhil V.
Etheridge, Joanne
Bourgeois, Laure
Zuo, Jian-Min
author_facet Nakashima, Philip N. H.
Shao, Yu-Tsun
Zhang, Zezhong
Smith, Andrew E.
Liu, Tianyu
Medhekar, Nikhil V.
Etheridge, Joanne
Bourgeois, Laure
Zuo, Jian-Min
contents All materials have defects and many contain nanostructures, both of which disrupt chemical bonding - the basis of materials properties. No experimental measurements of bonding electron distributions associated with defects and nanostructures have ever been possible. We present a method enabling such measurements and interrogate nanovoids surrounded by vacancies - the most fundamental of nanostructures and defects - in aluminium. We measure the volume of a vacancy with 3% uncertainty and map vacancy concentrations surrounding nanovoids with nanometre resolution in three dimensions where previously only two-dimensional mapping was possible. We discover that radiation-damaged voids can "heal". Our bonding measurements are depth-resolved, vacancy-sensitive, and agree with density functional theory. This work opens bonding electron density measurements to inhomogeneous nanostructured multi-phased materials so that the electronic origins of phenomena such as strengthening, weakening, interface functionality, solute diffusion and phase transformations within them may be revealed.
format Preprint
id arxiv_https___arxiv_org_abs_2512_05296
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle Mapping vacancy and bonding electron distributions around aluminium nanovoids
Nakashima, Philip N. H.
Shao, Yu-Tsun
Zhang, Zezhong
Smith, Andrew E.
Liu, Tianyu
Medhekar, Nikhil V.
Etheridge, Joanne
Bourgeois, Laure
Zuo, Jian-Min
Materials Science
Mesoscale and Nanoscale Physics
Applied Physics
Chemical Physics
Computational Physics
All materials have defects and many contain nanostructures, both of which disrupt chemical bonding - the basis of materials properties. No experimental measurements of bonding electron distributions associated with defects and nanostructures have ever been possible. We present a method enabling such measurements and interrogate nanovoids surrounded by vacancies - the most fundamental of nanostructures and defects - in aluminium. We measure the volume of a vacancy with 3% uncertainty and map vacancy concentrations surrounding nanovoids with nanometre resolution in three dimensions where previously only two-dimensional mapping was possible. We discover that radiation-damaged voids can "heal". Our bonding measurements are depth-resolved, vacancy-sensitive, and agree with density functional theory. This work opens bonding electron density measurements to inhomogeneous nanostructured multi-phased materials so that the electronic origins of phenomena such as strengthening, weakening, interface functionality, solute diffusion and phase transformations within them may be revealed.
title Mapping vacancy and bonding electron distributions around aluminium nanovoids
topic Materials Science
Mesoscale and Nanoscale Physics
Applied Physics
Chemical Physics
Computational Physics
url https://arxiv.org/abs/2512.05296