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Auteurs principaux: Ellis, Hunter, Duersch, Bobby G., Li, Botong, Rahaman, Imteaz, Pierce, Jim, Scarpulla, Michael A., Fu, Kai
Format: Preprint
Publié: 2025
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Accès en ligne:https://arxiv.org/abs/2512.12020
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_version_ 1866917144223023104
author Ellis, Hunter
Duersch, Bobby G.
Li, Botong
Rahaman, Imteaz
Pierce, Jim
Scarpulla, Michael A.
Fu, Kai
author_facet Ellis, Hunter
Duersch, Bobby G.
Li, Botong
Rahaman, Imteaz
Pierce, Jim
Scarpulla, Michael A.
Fu, Kai
contents NiO is a promising p-type material for photovoltaics and power electronics, but its temperature limits remain unclear. Using in situ high-temperature X-ray diffraction (HT-XRD) from 30 to 1100 C, we track the structural evolution of NiO thin films in air. The film crystallizes from an amorphous phase to cubic NiO between 300 and 400 C, where the emergence and growth of the (111) diffraction peak correlate with an increase in electrical resistivity. Further increases in temperature lead to improved crystallinity and higher resistivity. At 1100 C, the formation of Ni2O3 is observed, resulting in a highly resistive film. This study establishes a clear correlation between phase evolution, crystallinity, and resistive behavior in NiO thin films.
format Preprint
id arxiv_https___arxiv_org_abs_2512_12020
institution arXiv
publishDate 2025
record_format arxiv
spellingShingle In situ Study of p-NiO Film Quality at High Temperatures up to 1100 deg C
Ellis, Hunter
Duersch, Bobby G.
Li, Botong
Rahaman, Imteaz
Pierce, Jim
Scarpulla, Michael A.
Fu, Kai
Materials Science
NiO is a promising p-type material for photovoltaics and power electronics, but its temperature limits remain unclear. Using in situ high-temperature X-ray diffraction (HT-XRD) from 30 to 1100 C, we track the structural evolution of NiO thin films in air. The film crystallizes from an amorphous phase to cubic NiO between 300 and 400 C, where the emergence and growth of the (111) diffraction peak correlate with an increase in electrical resistivity. Further increases in temperature lead to improved crystallinity and higher resistivity. At 1100 C, the formation of Ni2O3 is observed, resulting in a highly resistive film. This study establishes a clear correlation between phase evolution, crystallinity, and resistive behavior in NiO thin films.
title In situ Study of p-NiO Film Quality at High Temperatures up to 1100 deg C
topic Materials Science
url https://arxiv.org/abs/2512.12020