A rapid low-background assay of $^{210}$Pb in archaeological lead

Fuente: arXiv
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Auteurs principaux: Consonni, M., Clemenza, M., Di Stefano, E., Iachellini, N. Ferreiro, Filippini, F., Gardini, A., Grosso, G., Pattavina, L., Della Pergola, R., Quitadamo, S., Sala, E., Saliu, F., Salvini, A., Trombetta, L.
Format: Preprint
Publié: 2026
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author Consonni, M.
Clemenza, M.
Di Stefano, E.
Iachellini, N. Ferreiro
Filippini, F.
Gardini, A.
Grosso, G.
Pattavina, L.
Della Pergola, R.
Quitadamo, S.
Sala, E.
Saliu, F.
Salvini, A.
Trombetta, L.
author_facet Consonni, M.
Clemenza, M.
Di Stefano, E.
Iachellini, N. Ferreiro
Filippini, F.
Gardini, A.
Grosso, G.
Pattavina, L.
Della Pergola, R.
Quitadamo, S.
Sala, E.
Saliu, F.
Salvini, A.
Trombetta, L.
contents In this work, we present a fast and highly efficient method for the measurement of $^{210}$Pb in metallic archaeological lead using the commercial low-background liquid scintillation counter Wallac Quantulus 1220 installed at the University of Milano-Bicocca (Italy). By combining an optimized chemical preparation with pulse-shape analysis (PSA), the technique achieves sensitivities at the level of a few $10^2$ mBq/kg within one week of measurement, using sample masses below 1 g. The method enables the simultaneous identification of the $β$ decays of $^{210}$Pb and $^{210}$Bi and the $α$ decay of $^{210}$Po, allowing a direct verification of secular equilibrium within the decay chain. With extended acquisition times, detection limits below 100 mBq/kg are reached after approximately 40 days. This approach provides a rapid, accessible, and reliable tool for the radiopurity screening of lead, and is well suited for quality control and R&D activities in next-generation low-background and rare-event physics experiments. Moreover, the method has the potential to be extended to other materials relevant for low-background applications.
format Preprint
id arxiv_https___arxiv_org_abs_2602_02674
institution arXiv
publishDate 2026
record_format arxiv
spellingShingle A rapid low-background assay of $^{210}$Pb in archaeological lead
Consonni, M.
Clemenza, M.
Di Stefano, E.
Iachellini, N. Ferreiro
Filippini, F.
Gardini, A.
Grosso, G.
Pattavina, L.
Della Pergola, R.
Quitadamo, S.
Sala, E.
Saliu, F.
Salvini, A.
Trombetta, L.
Instrumentation and Detectors
In this work, we present a fast and highly efficient method for the measurement of $^{210}$Pb in metallic archaeological lead using the commercial low-background liquid scintillation counter Wallac Quantulus 1220 installed at the University of Milano-Bicocca (Italy). By combining an optimized chemical preparation with pulse-shape analysis (PSA), the technique achieves sensitivities at the level of a few $10^2$ mBq/kg within one week of measurement, using sample masses below 1 g. The method enables the simultaneous identification of the $β$ decays of $^{210}$Pb and $^{210}$Bi and the $α$ decay of $^{210}$Po, allowing a direct verification of secular equilibrium within the decay chain. With extended acquisition times, detection limits below 100 mBq/kg are reached after approximately 40 days. This approach provides a rapid, accessible, and reliable tool for the radiopurity screening of lead, and is well suited for quality control and R&D activities in next-generation low-background and rare-event physics experiments. Moreover, the method has the potential to be extended to other materials relevant for low-background applications.
title A rapid low-background assay of $^{210}$Pb in archaeological lead
topic Instrumentation and Detectors
url https://arxiv.org/abs/2602.02674