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Main Authors: Un, Hio-Ieng, Orri, Jordi Ferrer, Jacobs, Ian E., Fukui, Naoya, Nishihara, Hiroshi, Ducati, Caterina, Stranks, Samuel D., Sirringhaus, Henning
Format: Preprint
Published: 2026
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Online Access:https://arxiv.org/abs/2603.00721
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author Un, Hio-Ieng
Orri, Jordi Ferrer
Jacobs, Ian E.
Fukui, Naoya
Nishihara, Hiroshi
Ducati, Caterina
Stranks, Samuel D.
Sirringhaus, Henning
author_facet Un, Hio-Ieng
Orri, Jordi Ferrer
Jacobs, Ian E.
Fukui, Naoya
Nishihara, Hiroshi
Ducati, Caterina
Stranks, Samuel D.
Sirringhaus, Henning
contents Understanding growth evolution and thereby implementing precise microstructural tuning of two-dimensional (2D) conjugated coordination polymers (cCPs) is crucial to achieve efficient electronic conduction towards their full potential and to observe materials' intrinsic properties. However, fundamental understanding of how 2D cCPs films grow remains very limited. Here, we use copper-benzenehexathiol (Cu-BHT) cCP as a model system to unravel the growth evolution of layered films in liquid-liquid interfacial synthesis in order to identify strategies to achieve tuning of structure-property relationships. We find that thin films formed at the early stage of growth in 20 minutes facilitate smoother, denser, and horizontally oriented films, and thereby achieve higher electrical conductivity of > 3000 S/cm with a metallic temperature dependence down to 20 K. They also reveal signatures of quantum interference mediated weak antilocalisation and Kondo-like effect in magnetotransport at low temperatures. These phenomena are not observed when long reaction time was employed. Our findings offer a new perspective for the growth of dynamically reversible self-assemblies, that is different from the traditional paradigm of longer reaction time being associated with higher ordering and performance, and offer a platform to study spin-related transport properties of these materials with higher performance for advanced electronic, thermoelectric, and potential spintronic applications.
format Preprint
id arxiv_https___arxiv_org_abs_2603_00721
institution arXiv
publishDate 2026
record_format arxiv
spellingShingle Controlling the growth of 2D conjugated coordination polymers to induce metallic and spin-dependent transport signatures
Un, Hio-Ieng
Orri, Jordi Ferrer
Jacobs, Ian E.
Fukui, Naoya
Nishihara, Hiroshi
Ducati, Caterina
Stranks, Samuel D.
Sirringhaus, Henning
Materials Science
Understanding growth evolution and thereby implementing precise microstructural tuning of two-dimensional (2D) conjugated coordination polymers (cCPs) is crucial to achieve efficient electronic conduction towards their full potential and to observe materials' intrinsic properties. However, fundamental understanding of how 2D cCPs films grow remains very limited. Here, we use copper-benzenehexathiol (Cu-BHT) cCP as a model system to unravel the growth evolution of layered films in liquid-liquid interfacial synthesis in order to identify strategies to achieve tuning of structure-property relationships. We find that thin films formed at the early stage of growth in 20 minutes facilitate smoother, denser, and horizontally oriented films, and thereby achieve higher electrical conductivity of > 3000 S/cm with a metallic temperature dependence down to 20 K. They also reveal signatures of quantum interference mediated weak antilocalisation and Kondo-like effect in magnetotransport at low temperatures. These phenomena are not observed when long reaction time was employed. Our findings offer a new perspective for the growth of dynamically reversible self-assemblies, that is different from the traditional paradigm of longer reaction time being associated with higher ordering and performance, and offer a platform to study spin-related transport properties of these materials with higher performance for advanced electronic, thermoelectric, and potential spintronic applications.
title Controlling the growth of 2D conjugated coordination polymers to induce metallic and spin-dependent transport signatures
topic Materials Science
url https://arxiv.org/abs/2603.00721