Multilayer Laue Lenses for Enhanced Spatial Resolution in Dark-Field X-ray Microscopy

Fuente: arXiv
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Autori principali: Staeck, Steffen, Yildirim, Can, Rodriguez-Lamas, Raquel, Dufrane, Thomas, Detlefs, Carsten, Gellert, Nis, Padula, Antonella Gayoso, Poulsen, Henning Friis
Natura: Preprint
Pubblicazione: 2026
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author Staeck, Steffen
Yildirim, Can
Rodriguez-Lamas, Raquel
Dufrane, Thomas
Detlefs, Carsten
Gellert, Nis
Padula, Antonella Gayoso
Poulsen, Henning Friis
author_facet Staeck, Steffen
Yildirim, Can
Rodriguez-Lamas, Raquel
Dufrane, Thomas
Detlefs, Carsten
Gellert, Nis
Padula, Antonella Gayoso
Poulsen, Henning Friis
contents We introduce the use of a crossed pair of Multilayer Laue Lenses (MLLs) as an objective in Dark-Field X-ray Microscopy (DFXM). In a demonstration experiment at the ID03 beamline at ESRF, two flat Mo-Si MLLs were used, with a physical aperture of 50 x 50 $\mathrm{μm^2}$ and a focal length of 14.25 mm at 19 keV. Applying a 10 % criterion to the Modulation Transfer Functions (MTFs) acquired, a spatial resolution of 56 nm is obtained in bright-field mode -- more than three times better than with a compound refractive lens (CRL) objective. The dark-field resolution is similar. With an efficiency of 26.7 % the MLL objective expands the science domain of DFXM significantly, both for bulk and near-surface studies. Similar to the CRL case, the reciprocal space resolution is dominated by the numerical aperture (NA) of the objective, with the NA being three times larger in the MLL case. This enables faster orientation mapping and implies improved options for the use of tomographic reconstruction algorithms. Although the MLL objective pupil varies with energy and position, secondary peaks are suppressed, simplifying both interpretation and forward simulations. We present an example DFXM application using the MLL as an objective, imaging a through-silicon via Kelvin device.
format Preprint
id arxiv_https___arxiv_org_abs_2604_20309
institution arXiv
publishDate 2026
record_format arxiv
spellingShingle Multilayer Laue Lenses for Enhanced Spatial Resolution in Dark-Field X-ray Microscopy
Staeck, Steffen
Yildirim, Can
Rodriguez-Lamas, Raquel
Dufrane, Thomas
Detlefs, Carsten
Gellert, Nis
Padula, Antonella Gayoso
Poulsen, Henning Friis
Materials Science
We introduce the use of a crossed pair of Multilayer Laue Lenses (MLLs) as an objective in Dark-Field X-ray Microscopy (DFXM). In a demonstration experiment at the ID03 beamline at ESRF, two flat Mo-Si MLLs were used, with a physical aperture of 50 x 50 $\mathrm{μm^2}$ and a focal length of 14.25 mm at 19 keV. Applying a 10 % criterion to the Modulation Transfer Functions (MTFs) acquired, a spatial resolution of 56 nm is obtained in bright-field mode -- more than three times better than with a compound refractive lens (CRL) objective. The dark-field resolution is similar. With an efficiency of 26.7 % the MLL objective expands the science domain of DFXM significantly, both for bulk and near-surface studies. Similar to the CRL case, the reciprocal space resolution is dominated by the numerical aperture (NA) of the objective, with the NA being three times larger in the MLL case. This enables faster orientation mapping and implies improved options for the use of tomographic reconstruction algorithms. Although the MLL objective pupil varies with energy and position, secondary peaks are suppressed, simplifying both interpretation and forward simulations. We present an example DFXM application using the MLL as an objective, imaging a through-silicon via Kelvin device.
title Multilayer Laue Lenses for Enhanced Spatial Resolution in Dark-Field X-ray Microscopy
topic Materials Science
url https://arxiv.org/abs/2604.20309