Tuning charge-transport properties and magnetic order in metallic EuTiO$_{3-δ}$

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Main Authors: He, Xing, Tan, Chiou Yang, Khayr, Issam, Van Fossan, Zach, Spieker, Richard J., Zhai, Dayu, Anderson, Sarah, Shukla, Dinesh, Sarker, Suchismita, Garcia-Barriocanal, Javier, Birol, Turan, Greven, Martin
Format: Preprint
Published: 2026
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author He, Xing
Tan, Chiou Yang
Khayr, Issam
Van Fossan, Zach
Spieker, Richard J.
Zhai, Dayu
Anderson, Sarah
Shukla, Dinesh
Sarker, Suchismita
Garcia-Barriocanal, Javier
Birol, Turan
Greven, Martin
author_facet He, Xing
Tan, Chiou Yang
Khayr, Issam
Van Fossan, Zach
Spieker, Richard J.
Zhai, Dayu
Anderson, Sarah
Shukla, Dinesh
Sarker, Suchismita
Garcia-Barriocanal, Javier
Birol, Turan
Greven, Martin
contents The stoichiometric antiferromagnetic insulator EuTiO$_3$ is proximate to a ferroelectric phase. Whereas cation substitution has been used as a tuning parameter to introduce charge carriers and manipulate the magnetism, the effects of oxygen-vacancy doping have been less explored. Here we report a detailed study of the charge transport and magnetic properties of metallic, oxygen-vacancy-doped EuTiO$_{3-δ}$. Using CaH$_2$ as an oxygen getter to achieve a higher carrier concentration than previously reported, we find that the phase diagram of the oxygen-vacancy-doped system is distinct from that obtained via cation doping. In particular, we uncover a change from antiferromagnetic to ferromagnetic order in the metallic state, with a maximum Curie temperature of TC $\approx$ 11 K at the highest carrier concentration of n $\approx$ 10$^{21}$ cm$^{-3}$. These findings are supported by density functional theory calculations, which indicate a significant change in the nearest-neighbor magnetic exchange constant with increasing electron doping. We also present x-ray diffuse scattering and complementary first-principles results that reveal that, similar to the prominent incipient ferroelectric perovskite SrTiO$_3$, the data for EuTiO$_3$ are consistent with thermal diffuse scattering and with the absence of quasi-elastic contributions. Finally, we report specific heat measurements that confirm the magnetic transition temperatures deduced from magnetization measurements and corroborate the lattice dynamics picture inferred from the diffuse scattering data.
format Preprint
id arxiv_https___arxiv_org_abs_2605_05612
institution arXiv
publishDate 2026
record_format arxiv
spellingShingle Tuning charge-transport properties and magnetic order in metallic EuTiO$_{3-δ}$
He, Xing
Tan, Chiou Yang
Khayr, Issam
Van Fossan, Zach
Spieker, Richard J.
Zhai, Dayu
Anderson, Sarah
Shukla, Dinesh
Sarker, Suchismita
Garcia-Barriocanal, Javier
Birol, Turan
Greven, Martin
Materials Science
The stoichiometric antiferromagnetic insulator EuTiO$_3$ is proximate to a ferroelectric phase. Whereas cation substitution has been used as a tuning parameter to introduce charge carriers and manipulate the magnetism, the effects of oxygen-vacancy doping have been less explored. Here we report a detailed study of the charge transport and magnetic properties of metallic, oxygen-vacancy-doped EuTiO$_{3-δ}$. Using CaH$_2$ as an oxygen getter to achieve a higher carrier concentration than previously reported, we find that the phase diagram of the oxygen-vacancy-doped system is distinct from that obtained via cation doping. In particular, we uncover a change from antiferromagnetic to ferromagnetic order in the metallic state, with a maximum Curie temperature of TC $\approx$ 11 K at the highest carrier concentration of n $\approx$ 10$^{21}$ cm$^{-3}$. These findings are supported by density functional theory calculations, which indicate a significant change in the nearest-neighbor magnetic exchange constant with increasing electron doping. We also present x-ray diffuse scattering and complementary first-principles results that reveal that, similar to the prominent incipient ferroelectric perovskite SrTiO$_3$, the data for EuTiO$_3$ are consistent with thermal diffuse scattering and with the absence of quasi-elastic contributions. Finally, we report specific heat measurements that confirm the magnetic transition temperatures deduced from magnetization measurements and corroborate the lattice dynamics picture inferred from the diffuse scattering data.
title Tuning charge-transport properties and magnetic order in metallic EuTiO$_{3-δ}$
topic Materials Science
url https://arxiv.org/abs/2605.05612