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Autori principali: Anzivino, Barbara, Tilley, Leon J., Ingalls, Laura R., Hall, Adam B., Drugan, John E.
Natura: Recurso educativo Open Access
Lingua:en
Pubblicazione: 2009
Soggetti:
Accesso online:https://eric.ed.gov/?id=EJ838932
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author Anzivino, Barbara
Tilley, Leon J.
Ingalls, Laura R.
Hall, Adam B.
Drugan, John E.
author_facet Anzivino, Barbara
Tilley, Leon J.
Ingalls, Laura R.
Hall, Adam B.
Drugan, John E.
Anzivino, Barbara
Tilley, Leon J.
Ingalls, Laura R.
Hall, Adam B.
Drugan, John E.
collection Education Resources Information Center
contents Got a Match? Ion Extraction GC-MS Characterization of Accelerants Adsorbed in Charcoal Using Negative Pressure Dynamic Headspace Concentration Anzivino, Barbara Tilley, Leon J. Ingalls, Laura R. Hall, Adam B. Drugan, John E. Organic Chemistry Classification Anxiety College Science Undergraduate Study Crime Science Laboratories Laboratory Experiments Spectroscopy Molecular Structure Heat Scientific Principles An undergraduate organic chemistry experiment demonstrating real-life application of GC-MS to arson accelerant identification is described. Students are given the task of comparing a sample recovered from a "crime scene" to that from a "suspect's clothing". Accelerants subjected to different conditions are recovered using a quick and simple negative pressure dynamic headspace method. GC-MS data is acquired. Students apply ion-extraction techniques and spectral library searches in conjunction with mass spectral fragmentation pattern analyses to classify accelerants according to an ignitable liquid classification scheme similar to that used by the American Society for Testing and Materials. After classification, they are asked to make a determination about the degree (or lack thereof) of match between samples and address several critical thinking issues regarding a suspect's possible innocence or guilt. (Contains 8 figures and 2 tables.)
format Recurso educativo Open Access
id eric_EJ838932
institution ERIC Institute of Education Sciences
language en
publishDate 2009
record_format eric
spellingShingle Got a Match? Ion Extraction GC-MS Characterization of Accelerants Adsorbed in Charcoal Using Negative Pressure Dynamic Headspace Concentration
Anzivino, Barbara
Tilley, Leon J.
Ingalls, Laura R.
Hall, Adam B.
Drugan, John E.
Organic Chemistry
Classification
Anxiety
College Science
Undergraduate Study
Crime
Science Laboratories
Laboratory Experiments
Spectroscopy
Molecular Structure
Heat
Scientific Principles
Got a Match? Ion Extraction GC-MS Characterization of Accelerants Adsorbed in Charcoal Using Negative Pressure Dynamic Headspace Concentration Anzivino, Barbara Tilley, Leon J. Ingalls, Laura R. Hall, Adam B. Drugan, John E. Organic Chemistry Classification Anxiety College Science Undergraduate Study Crime Science Laboratories Laboratory Experiments Spectroscopy Molecular Structure Heat Scientific Principles An undergraduate organic chemistry experiment demonstrating real-life application of GC-MS to arson accelerant identification is described. Students are given the task of comparing a sample recovered from a "crime scene" to that from a "suspect's clothing". Accelerants subjected to different conditions are recovered using a quick and simple negative pressure dynamic headspace method. GC-MS data is acquired. Students apply ion-extraction techniques and spectral library searches in conjunction with mass spectral fragmentation pattern analyses to classify accelerants according to an ignitable liquid classification scheme similar to that used by the American Society for Testing and Materials. After classification, they are asked to make a determination about the degree (or lack thereof) of match between samples and address several critical thinking issues regarding a suspect's possible innocence or guilt. (Contains 8 figures and 2 tables.)
title Got a Match? Ion Extraction GC-MS Characterization of Accelerants Adsorbed in Charcoal Using Negative Pressure Dynamic Headspace Concentration
topic Organic Chemistry
Classification
Anxiety
College Science
Undergraduate Study
Crime
Science Laboratories
Laboratory Experiments
Spectroscopy
Molecular Structure
Heat
Scientific Principles
url https://eric.ed.gov/?id=EJ838932