Disaggregated indurated carbonate samples using Calgon, acetic acid and electric pulse fragmentation

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Autori principali: Beasley, Charlotte, Parvaz, Daniel B, Cotton, Laura, Littler, Kate
Natura: Dataset Open Access
Lingua:en
Pubblicazione: PANGAEA 2021
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author Beasley, Charlotte
Parvaz, Daniel B
Cotton, Laura
Littler, Kate
author_facet Beasley, Charlotte
Parvaz, Daniel B
Cotton, Laura
Littler, Kate
collection Datos científicos de ciencias marinas y ambientales
contents Three disaggregation methods, i.e. Calgon, acetic acid and electric pulse fragmentation (EPF), have been applied to a range of heavily lithified, carbonate-rich sedimentary rock samples of Paleogene age. Samples are predominantly from the carbonate-rich, shallow water domain (< 250m palaeo-water depth) of Tanzania, Malta and the United Arab Emirates (Paleogene Tethys Ocean). The effectiveness and efficiency of each method has been compared, in addition to the preservation of the resultant liberated microfossil material (primarily larger foraminifera; LF). Of the three methods, the most efficient and effective was EPF, which liberated the largest number of LF in a very short processing time and resulted in the best preservation. Samples with calcitic, silicic, and clay matrices and cements were successfully disaggregated using EPF. In this study, recovered microfossils were largely > 500 μm, suggesting this technique may be more appropriate for liberating larger microfossils (e.g. LFs); however, we discuss nuances to the method that would allow for more effective recovery of smaller microfossil specimens. The more traditional acetic acid method was also able to disaggregate a number of the samples; however, preservation of the LF was compromised. We suggest a best-practice methodology for implementing EPF in micropalaeontological studies.
format Dataset Open Access
id pangaea_https___doi_org_10_1594_PANGAEA_927054
institution PANGAEA
language en
publishDate 2021
publisher PANGAEA
record_format pangaea
spellingShingle Disaggregated indurated carbonate samples using Calgon, acetic acid and electric pulse fragmentation
Beasley, Charlotte
Parvaz, Daniel B
Cotton, Laura
Littler, Kate
carbonates; disaggregation; electric pulse fragmentation
Three disaggregation methods, i.e. Calgon, acetic acid and electric pulse fragmentation (EPF), have been applied to a range of heavily lithified, carbonate-rich sedimentary rock samples of Paleogene age. Samples are predominantly from the carbonate-rich, shallow water domain (< 250m palaeo-water depth) of Tanzania, Malta and the United Arab Emirates (Paleogene Tethys Ocean). The effectiveness and efficiency of each method has been compared, in addition to the preservation of the resultant liberated microfossil material (primarily larger foraminifera; LF). Of the three methods, the most efficient and effective was EPF, which liberated the largest number of LF in a very short processing time and resulted in the best preservation. Samples with calcitic, silicic, and clay matrices and cements were successfully disaggregated using EPF. In this study, recovered microfossils were largely > 500 μm, suggesting this technique may be more appropriate for liberating larger microfossils (e.g. LFs); however, we discuss nuances to the method that would allow for more effective recovery of smaller microfossil specimens. The more traditional acetic acid method was also able to disaggregate a number of the samples; however, preservation of the LF was compromised. We suggest a best-practice methodology for implementing EPF in micropalaeontological studies.
title Disaggregated indurated carbonate samples using Calgon, acetic acid and electric pulse fragmentation
topic carbonates; disaggregation; electric pulse fragmentation
url https://doi.org/10.1594/PANGAEA.927054