Blank masses for individual polychlorinated biphenyl congeners in soils from East Chicago, Indiana, USA in 2017/2018

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Main Authors: Martinez, Andres, Hua, Jason, Haque, Ezazul, Thorne, Peter, Hornbuckle, Keri C
Format: Dataset Open Access
Language:en
Published: PANGAEA 2022
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author Martinez, Andres
Hua, Jason
Haque, Ezazul
Thorne, Peter
Hornbuckle, Keri C
author_facet Martinez, Andres
Hua, Jason
Haque, Ezazul
Thorne, Peter
Hornbuckle, Keri C
collection Datos científicos de ciencias marinas y ambientales
contents Combusted diatomaceous earth (DE, Thermo Fisher Scientific) was used as method blank. A total of 8 method blanks (one blank per sample batch), were included during extraction, clean up and quantification of the samples. Gas chromatography (GC) in tandem with Mass Spectrometry GC-MS/MS (Agilent 7000) in multiple reaction monitoring (MRM) mode was used to quantify all 209 congeners in 171 individual or coeluting congener peaks. The GC was equipped with a Supelco SBP-Octyl capillary column (30 m × 0.25 mm ID, 0.25 mm film thicknesses) with helium as carrier gas.
format Dataset Open Access
id pangaea_https___doi_org_10_1594_PANGAEA_941686
institution PANGAEA
language en
publishDate 2022
publisher PANGAEA
record_format pangaea
spellingShingle Blank masses for individual polychlorinated biphenyl congeners in soils from East Chicago, Indiana, USA in 2017/2018
Martinez, Andres
Hua, Jason
Haque, Ezazul
Thorne, Peter
Hornbuckle, Keri C
Blank sample (diatomaceous earth); Date/time end; Date/time start; EastChicago_DE_BM1; EastChicago_DE_BM2; EastChicago_DE_BM3; EastChicago_DE_BM4; EastChicago_DE_BM5; EastChicago_DE_BM6; EastChicago_DE_BM7; EastChicago_DE_BM8; East Chicago, Indiana, USA; Event label; LATITUDE; LONGITUDE; Method comment; PCB congeners; Polychlorinated biphenyl, per unit diatomaceous earth; Sample code/label; Soil; tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM); TOC
Combusted diatomaceous earth (DE, Thermo Fisher Scientific) was used as method blank. A total of 8 method blanks (one blank per sample batch), were included during extraction, clean up and quantification of the samples. Gas chromatography (GC) in tandem with Mass Spectrometry GC-MS/MS (Agilent 7000) in multiple reaction monitoring (MRM) mode was used to quantify all 209 congeners in 171 individual or coeluting congener peaks. The GC was equipped with a Supelco SBP-Octyl capillary column (30 m × 0.25 mm ID, 0.25 mm film thicknesses) with helium as carrier gas.
title Blank masses for individual polychlorinated biphenyl congeners in soils from East Chicago, Indiana, USA in 2017/2018
topic Blank sample (diatomaceous earth); Date/time end; Date/time start; EastChicago_DE_BM1; EastChicago_DE_BM2; EastChicago_DE_BM3; EastChicago_DE_BM4; EastChicago_DE_BM5; EastChicago_DE_BM6; EastChicago_DE_BM7; EastChicago_DE_BM8; East Chicago, Indiana, USA; Event label; LATITUDE; LONGITUDE; Method comment; PCB congeners; Polychlorinated biphenyl, per unit diatomaceous earth; Sample code/label; Soil; tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM); TOC
url https://doi.org/10.1594/PANGAEA.941686