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author Reis, Alex
Fichtner, Vanessa
Erhardt, Andrea M
author_facet Reis, Alex
Fichtner, Vanessa
Erhardt, Andrea M
collection Datos científicos de ciencias marinas y ambientales
contents Dissolved sulfate sulfur and oxygen isotope results and carbonate associated sulfate sulfur isotope results from IODP Site U1553 (166°11.4801′E, 52°13.4294′S) located on the Campbell Plateau are presented. Pore water collected during IODP Expedition 378 at Site U1553 in January 2020 were used for this study. These samples were processed using a procedure modified from that in Wotte et al. (2012, doi:10.1016/j.gca.2012.02.013) to extract the sulfate from the aqueous phase. The dissolved sulfate in the pore water was extracted by first adding 10% HCl to acidify the pore water, then the sulfate was removed from solution as barium sulfate using a 10% BaCl2 solution. Sulfur isotopes in dissolved sulfate were analyzed using an EA-Isolink elemental analyzer connected in continuous flow to a MAT253 IRMS and the oxygen isotopes in dissolved sulfate were measured using a thermal conversion elemental analyzer connected in continuous flow to a Delta V IRMS. Analytical precision was measured using repeated measurements of a blind standard with an average 2-sigma of 0.4‰ for sulfur isotopes (IAEA-SO-5) and 0.3‰ for oxygen isotopes (NBS-127). These data were collected to examine the impact of a long-duration (~26-million-year) unconformity has on the fidelity of the carbonate geochemical archive.
format Dataset Open Access
id pangaea_https___doi_org_10_1594_PANGAEA_959571
institution PANGAEA
language en
publishDate 2023
publisher PANGAEA
record_format pangaea
spellingShingle Sulfur and Oxygen Isotopic Composition of Dissolved Sulfate in Interstitial Water Sample Residues from IODP Site U1553 on the southern Campbell Plateau
Reis, Alex
Fichtner, Vanessa
Erhardt, Andrea M
378-U1553A; 378-U1553B; 378-U1553C; Date/Time of event; Depth, bottom/max; DEPTH, sediment/rock; Depth, top/min; DRILL; Drilling/drill rig; DSDP/ODP/IODP sample designation; Event label; Exp378; Isotope ratio mass spectrometer (IRMS), Thermo Fisher, Delta Plus; coupled with Universal continuous flow interface, Thermo Fisher, Conflo II; coupled with Isotope Ratio Mass Spectrometer, Thermo Fisher, Delta Plus; Isotope ratio mass spectrometer (IRMS), Thermo Fisher, MAT253; coupled with Universal continuous flow interface, Thermo Fisher, Conflo IV; coupled with Elemental Analyzer, Thermo Fisher, EA-Isolink; Joides Resolution; Latitude of event; Longitude of event; Oxygen isotopes; Paleoceanography; Sample code/label; South Pacific Ocean; Sulfur isotopes; δ18O, sulfate; δ18O, sulfate, standard deviation; δ34S, sulfate
Dissolved sulfate sulfur and oxygen isotope results and carbonate associated sulfate sulfur isotope results from IODP Site U1553 (166°11.4801′E, 52°13.4294′S) located on the Campbell Plateau are presented. Pore water collected during IODP Expedition 378 at Site U1553 in January 2020 were used for this study. These samples were processed using a procedure modified from that in Wotte et al. (2012, doi:10.1016/j.gca.2012.02.013) to extract the sulfate from the aqueous phase. The dissolved sulfate in the pore water was extracted by first adding 10% HCl to acidify the pore water, then the sulfate was removed from solution as barium sulfate using a 10% BaCl2 solution. Sulfur isotopes in dissolved sulfate were analyzed using an EA-Isolink elemental analyzer connected in continuous flow to a MAT253 IRMS and the oxygen isotopes in dissolved sulfate were measured using a thermal conversion elemental analyzer connected in continuous flow to a Delta V IRMS. Analytical precision was measured using repeated measurements of a blind standard with an average 2-sigma of 0.4‰ for sulfur isotopes (IAEA-SO-5) and 0.3‰ for oxygen isotopes (NBS-127). These data were collected to examine the impact of a long-duration (~26-million-year) unconformity has on the fidelity of the carbonate geochemical archive.
title Sulfur and Oxygen Isotopic Composition of Dissolved Sulfate in Interstitial Water Sample Residues from IODP Site U1553 on the southern Campbell Plateau
topic 378-U1553A; 378-U1553B; 378-U1553C; Date/Time of event; Depth, bottom/max; DEPTH, sediment/rock; Depth, top/min; DRILL; Drilling/drill rig; DSDP/ODP/IODP sample designation; Event label; Exp378; Isotope ratio mass spectrometer (IRMS), Thermo Fisher, Delta Plus; coupled with Universal continuous flow interface, Thermo Fisher, Conflo II; coupled with Isotope Ratio Mass Spectrometer, Thermo Fisher, Delta Plus; Isotope ratio mass spectrometer (IRMS), Thermo Fisher, MAT253; coupled with Universal continuous flow interface, Thermo Fisher, Conflo IV; coupled with Elemental Analyzer, Thermo Fisher, EA-Isolink; Joides Resolution; Latitude of event; Longitude of event; Oxygen isotopes; Paleoceanography; Sample code/label; South Pacific Ocean; Sulfur isotopes; δ18O, sulfate; δ18O, sulfate, standard deviation; δ34S, sulfate
url https://doi.org/10.1594/PANGAEA.959571