δ Deuterium leaf wax isotopes from sediment core of Lake Alchichica in Mexico

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Autori principali: Safaierad, Reza, Israde-Alcántara, Isabel, Rantala, Marttiina V, Domínguez-Vázquez, Gabriela, Schefuß, Enno, Tylmann, Wojciech, Francus, Pierre, Mattielli, Nadine, Metcalfe, Sarah, Fagel, Nathalie
Natura: Dataset Open Access
Lingua:en
Pubblicazione: PANGAEA 2026
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author Safaierad, Reza
Israde-Alcántara, Isabel
Rantala, Marttiina V
Domínguez-Vázquez, Gabriela
Schefuß, Enno
Tylmann, Wojciech
Francus, Pierre
Mattielli, Nadine
Metcalfe, Sarah
Fagel, Nathalie
author_facet Safaierad, Reza
Israde-Alcántara, Isabel
Rantala, Marttiina V
Domínguez-Vázquez, Gabriela
Schefuß, Enno
Tylmann, Wojciech
Francus, Pierre
Mattielli, Nadine
Metcalfe, Sarah
Fagel, Nathalie
collection Datos científicos de ciencias marinas y ambientales
contents The isotope analyses were performed on subsamples from a 57-cm-long sediment core retrieved from Lake Alchichica (19° 24' 38 N, 97° 24' 14 W, 2322 masl) at a water depth of ~ 60 m using a Uwitec® coring device equipped with a 9-cm coring tube. n-alkanes were extracted from 20 dried samples (1.3–2.8 g) using DCM:MeOH (9:1) in a DIONEX ASE-200 at 100°C and 1000 psi for 5 minutes, repeated thrice, with squalane as an internal standard. Lipid extracts were concentrated under N₂, treated with activated copper to remove sulfur, and saponified with 6% KOH in MeOH at 80°C for 2 hours. Hydrocarbons, ketones, and alcohols were extracted with hexane, and non-polar hydrocarbons were isolated using silica gel and silver nitrate-silica columns. Saturated fractions were analyzed by GC/FID at MARUM, University of Bremen, with retention time comparison for compound identification and <5% quantification precision.
format Dataset Open Access
id pangaea_https___doi_org_10_1594_PANGAEA_982935
institution PANGAEA
language en
publishDate 2026
publisher PANGAEA
record_format pangaea
spellingShingle δ Deuterium leaf wax isotopes from sediment core of Lake Alchichica in Mexico
Safaierad, Reza
Israde-Alcántara, Isabel
Rantala, Marttiina V
Domínguez-Vázquez, Gabriela
Schefuß, Enno
Tylmann, Wojciech
Francus, Pierre
Mattielli, Nadine
Metcalfe, Sarah
Fagel, Nathalie
AGE; Age, Bayesian based model Plum on Pb-210 and C-14 data; carbon isotope; DEPTH, sediment/rock; Deuterium Isotopes; Gas chromatography - Flame Ionization Detection (GC-FID); Lake_Alchichica; leaf waxes; Mexico; oxygen isotope; Pollen; Sediment core; Sediment corer, UWITEC; XRD; XRF core scanner data; δ Deuterium, wax; δ Deuterium, wax, standard deviation
The isotope analyses were performed on subsamples from a 57-cm-long sediment core retrieved from Lake Alchichica (19° 24' 38 N, 97° 24' 14 W, 2322 masl) at a water depth of ~ 60 m using a Uwitec® coring device equipped with a 9-cm coring tube. n-alkanes were extracted from 20 dried samples (1.3–2.8 g) using DCM:MeOH (9:1) in a DIONEX ASE-200 at 100°C and 1000 psi for 5 minutes, repeated thrice, with squalane as an internal standard. Lipid extracts were concentrated under N₂, treated with activated copper to remove sulfur, and saponified with 6% KOH in MeOH at 80°C for 2 hours. Hydrocarbons, ketones, and alcohols were extracted with hexane, and non-polar hydrocarbons were isolated using silica gel and silver nitrate-silica columns. Saturated fractions were analyzed by GC/FID at MARUM, University of Bremen, with retention time comparison for compound identification and <5% quantification precision.
title δ Deuterium leaf wax isotopes from sediment core of Lake Alchichica in Mexico
topic AGE; Age, Bayesian based model Plum on Pb-210 and C-14 data; carbon isotope; DEPTH, sediment/rock; Deuterium Isotopes; Gas chromatography - Flame Ionization Detection (GC-FID); Lake_Alchichica; leaf waxes; Mexico; oxygen isotope; Pollen; Sediment core; Sediment corer, UWITEC; XRD; XRF core scanner data; δ Deuterium, wax; δ Deuterium, wax, standard deviation
url https://doi.org/10.1594/PANGAEA.982935