Blanks for microlitter samples from tropical to temperate regions of the Atlantic Ocean

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Auteurs principaux: Birnstiel, Stéphanie, Grelaud, Michaël, Teixeira, Carlos E P, Guilherme, Andreia, Lorenz, Claudia, Vollertsen, Jes, Sobral, Paula, Langer, Gerald, Ziveri, Patrizia
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Langue:en
Publié: PANGAEA 2026
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author Birnstiel, Stéphanie
Grelaud, Michaël
Teixeira, Carlos E P
Guilherme, Andreia
Lorenz, Claudia
Vollertsen, Jes
Sobral, Paula
Langer, Gerald
Ziveri, Patrizia
author_facet Birnstiel, Stéphanie
Grelaud, Michaël
Teixeira, Carlos E P
Guilherme, Andreia
Lorenz, Claudia
Vollertsen, Jes
Sobral, Paula
Langer, Gerald
Ziveri, Patrizia
collection Datos científicos de ciencias marinas y ambientales
contents Sampling was performed during the PYROWIND oceanographic campaign in the Atlantic Ocean (April 27th – May 19th 2022), on board of the Spanish R/V Hespérides. The research cruise covered an 8,000-km transect, from Brazil (Salvador) to the Strait of Gibraltar. Subsurface water samples (n = 52) were continuously collected through the pump-underway ship intake system during navigation. Field and procedural blanks were introduced to assess possible sample contamination. In the field, a petri dish with a polycarbonate filter (0.45 μm) was left open at the working station (field blank) for each set of samples to assess airborne contamination (n = 52). The blank remained open during the duration of the samples' preparation and removal. Procedural blanks (all reagents and materials with no sample; 1 blank per 10 samples) were run parallelly to the samples, following the same steps. Particles were quantified and analyzed using ATR-FTIR (≥ 315 μm) and μFTIR (10–315 μm). The large fraction (≥ 315 μm) was analyzed on a stereomicroscope (Leica Z16 APO) equipped with a camera (Canon EOS 650D). The filter was horizontally examined from the top left to the bottom right and every relevant particle was photographed. Each particle was counted and classified according to their type. The chemical analysis was carried out using ATR-FTIR (Agilent 630 Cary ATR-FTIR spectroscopy). The small fraction (10–315 μm) was analyzed using μFTIR (Agilent 620 FTIR microscope with a FPA detector and a Cary 670 FTIR spectrometer) and examined with siMPle (Primpke et al., 2020).
format Dataset Open Access
id pangaea_https___doi_org_10_1594_PANGAEA_986744
institution PANGAEA
language en
publishDate 2026
publisher PANGAEA
record_format pangaea
spellingShingle Blanks for microlitter samples from tropical to temperate regions of the Atlantic Ocean
Birnstiel, Stéphanie
Grelaud, Michaël
Teixeira, Carlos E P
Guilherme, Andreia
Lorenz, Claudia
Vollertsen, Jes
Sobral, Paula
Langer, Gerald
Ziveri, Patrizia
Acrylic particles; Atlantic Ocean; Blank; cellulosic fibers; Cellulosic fibres; continuous sampling; Fibres; Films; Fragments; JPI Oceans - i-plastic; JPIO-i-plastic; microlitter; Microplastics; Polyethylene; Polyethylene terephthalate; Polypropylene; Polystyrene; Polyurethane; Polyvinyl alcohol; subsurface waters; Underway measurement
Sampling was performed during the PYROWIND oceanographic campaign in the Atlantic Ocean (April 27th – May 19th 2022), on board of the Spanish R/V Hespérides. The research cruise covered an 8,000-km transect, from Brazil (Salvador) to the Strait of Gibraltar. Subsurface water samples (n = 52) were continuously collected through the pump-underway ship intake system during navigation. Field and procedural blanks were introduced to assess possible sample contamination. In the field, a petri dish with a polycarbonate filter (0.45 μm) was left open at the working station (field blank) for each set of samples to assess airborne contamination (n = 52). The blank remained open during the duration of the samples' preparation and removal. Procedural blanks (all reagents and materials with no sample; 1 blank per 10 samples) were run parallelly to the samples, following the same steps. Particles were quantified and analyzed using ATR-FTIR (≥ 315 μm) and μFTIR (10–315 μm). The large fraction (≥ 315 μm) was analyzed on a stereomicroscope (Leica Z16 APO) equipped with a camera (Canon EOS 650D). The filter was horizontally examined from the top left to the bottom right and every relevant particle was photographed. Each particle was counted and classified according to their type. The chemical analysis was carried out using ATR-FTIR (Agilent 630 Cary ATR-FTIR spectroscopy). The small fraction (10–315 μm) was analyzed using μFTIR (Agilent 620 FTIR microscope with a FPA detector and a Cary 670 FTIR spectrometer) and examined with siMPle (Primpke et al., 2020).
title Blanks for microlitter samples from tropical to temperate regions of the Atlantic Ocean
topic Acrylic particles; Atlantic Ocean; Blank; cellulosic fibers; Cellulosic fibres; continuous sampling; Fibres; Films; Fragments; JPI Oceans - i-plastic; JPIO-i-plastic; microlitter; Microplastics; Polyethylene; Polyethylene terephthalate; Polypropylene; Polystyrene; Polyurethane; Polyvinyl alcohol; subsurface waters; Underway measurement
url https://doi.org/10.1594/PANGAEA.986744