SYNTHESIS AND CHARACTERIZATION OF CALCIUM PHOSPHATE AND ITS RELATION TO CR(VI) ADSORPTION PROPERTIES

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Main Author: Francisco GRANADOS-CORREA
Format: Artículo científico
Language:en
Published: Universidad Nacional Autónoma de México 2010
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author Francisco GRANADOS-CORREA
author_facet Francisco GRANADOS-CORREA
contents SYNTHESIS AND CHARACTERIZATION OF CALCIUM PHOSPHATE AND ITS RELATION TO CR(VI) ADSORPTION PROPERTIES Francisco GRANADOS-CORREA Juan BONIFACIO-MARTÍNEZ Juan SERRANO-GÓMEZ Ciencias de la Tierra synthesis surface area characterization Calcium phosphate Cr(VI) adsorption Calcium phosphate with hydroxyapatite structure was synthesized and its ability to adsorb Cr(VI) from aqueous solution is presented. XRD, BET, IR, TGA, SEM and EDS techniques were used to characterize the obtained material. A pure phase was obtained through a simple synthesis process. The specific surface area of the synthesized powder was found to be 64.5 m2 g-1. The X-ray diffraction pattern shows that the calcium phosphate formed was nanocrystalline with an average grain size of approximately 75 nm. A fast adsorption was observed and in less than 24 h it was found that 2.41 x 10-4 meq g-1 of Cr(VI) ions were adsorbed on calcium phosphate. Desorption experiments showed that Cr(VI) adsorption decreased to 2.23 x 10-4 meq g-1 of calcium phosphate. This behavior is a consequence of partial dehydration of the synthesized material. Calcium phosphate can be effectively used for removing Cr(VI) from aqueous solutions in treatment processes of metal wastes. 2010 artículo científico 0188-4999 https://www.redalyc.org/articulo.oa?id=37014383004 en http://www.redalyc.org/revista.oa?id=370 Revista Internacional de Contaminación Ambiental application/pdf Universidad Nacional Autónoma de México Revista Internacional de Contaminación Ambiental (México) Num.2 Vol.26
format Artículo científico
id redalyc_37014383004
institution Redalyc
language en
publishDate 2010
publisher Universidad Nacional Autónoma de México
spellingShingle SYNTHESIS AND CHARACTERIZATION OF CALCIUM PHOSPHATE AND ITS RELATION TO CR(VI) ADSORPTION PROPERTIES
Francisco GRANADOS-CORREA
Ciencias de la Tierra
synthesis
surface area
characterization
Calcium phosphate
Cr(VI) adsorption
SYNTHESIS AND CHARACTERIZATION OF CALCIUM PHOSPHATE AND ITS RELATION TO CR(VI) ADSORPTION PROPERTIES Francisco GRANADOS-CORREA Juan BONIFACIO-MARTÍNEZ Juan SERRANO-GÓMEZ Ciencias de la Tierra synthesis surface area characterization Calcium phosphate Cr(VI) adsorption Calcium phosphate with hydroxyapatite structure was synthesized and its ability to adsorb Cr(VI) from aqueous solution is presented. XRD, BET, IR, TGA, SEM and EDS techniques were used to characterize the obtained material. A pure phase was obtained through a simple synthesis process. The specific surface area of the synthesized powder was found to be 64.5 m2 g-1. The X-ray diffraction pattern shows that the calcium phosphate formed was nanocrystalline with an average grain size of approximately 75 nm. A fast adsorption was observed and in less than 24 h it was found that 2.41 x 10-4 meq g-1 of Cr(VI) ions were adsorbed on calcium phosphate. Desorption experiments showed that Cr(VI) adsorption decreased to 2.23 x 10-4 meq g-1 of calcium phosphate. This behavior is a consequence of partial dehydration of the synthesized material. Calcium phosphate can be effectively used for removing Cr(VI) from aqueous solutions in treatment processes of metal wastes. 2010 artículo científico 0188-4999 https://www.redalyc.org/articulo.oa?id=37014383004 en http://www.redalyc.org/revista.oa?id=370 Revista Internacional de Contaminación Ambiental application/pdf Universidad Nacional Autónoma de México Revista Internacional de Contaminación Ambiental (México) Num.2 Vol.26
title SYNTHESIS AND CHARACTERIZATION OF CALCIUM PHOSPHATE AND ITS RELATION TO CR(VI) ADSORPTION PROPERTIES
topic Ciencias de la Tierra
synthesis
surface area
characterization
Calcium phosphate
Cr(VI) adsorption
url https://www.redalyc.org/articulo.oa?id=37014383004