Mechanical and tribological properties enhancement of heat treated AISI 4340 steel by using a TiN/TiAlN multilayer coating system

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Autore principale: Gilberto Bejarano
Natura: Artículo científico
Lingua:en
Pubblicazione: Universidad de Antioquia 2008
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author Gilberto Bejarano
author_facet Gilberto Bejarano
contents Mechanical and tribological properties enhancement of heat treated AISI 4340 steel by using a TiN/TiAlN multilayer coating system Gilberto Bejarano Julio Caicedo Juan Muñoz Saldaña Ingeniería TiN hard coatings TiAlN coatings multilayer system Magnetron sputtering TiN/TiAlN (titanium nitride/titanium aluminum nitride) multilayer were deposited by d.c. reactive magnetron sputtering using titanium and aluminum targets with 10 cm in diameter and 99.9% purity in an argon/nitrogen (Ar/N) atmosphere, applying a substrate temperature of 300°C and a pressure of 7x10-3 mbar. Silicon (100) and heat treated AISI 4340 steel samples with a hardness of 54 Rockwell C (HRC, approximately 5.4 GPa) were utilized as substrate. TiN/TiAlN coatings with 70% aluminum and 4 um total thickness were investigated as function of multilayer number and their mechanical and tribological properties compared to the uncoated steel samples. The crystalline structure of the coated samples was analyzed through X-ray diffractometry and its morphology and topography using scanning electron microscopy (SEM) and atomic force microscopy (AFM). Hardness was determined by means of nanoindentation, while wear resistance was characterized through pin on disc measurements. A hardness and Young Modulus increment from 62% and 70% respectively, were obtained for 150 multilayer of TiN/TiAlN related to 30 bilayers and from 740% and 202% respectively, compared with the uncoated AISI 4340 steel samples. Finally the friction coefficient was reduced from 0.55 down to 0.20 and the roughness from 63 nm to 3.2 nm for the steel samples coated with 150 bilayers of TiN/TiAlN, what conduced to a greater wear resistance of the coating system. 2008 artículo científico 0120-6230 https://www.redalyc.org/articulo.oa?id=43004405 en http://www.redalyc.org/revista.oa?id=430 Revista Facultad de Ingeniería Universidad de Antioquia application/pdf Universidad de Antioquia Revista Facultad de Ingeniería Universidad de Antioquia (Colombia) Num.44
format Artículo científico
id redalyc_43004405
institution Redalyc
language en
publishDate 2008
publisher Universidad de Antioquia
spellingShingle Mechanical and tribological properties enhancement of heat treated AISI 4340 steel by using a TiN/TiAlN multilayer coating system
Gilberto Bejarano
Ingeniería
TiN
hard coatings
TiAlN coatings
multilayer system
Magnetron sputtering
Mechanical and tribological properties enhancement of heat treated AISI 4340 steel by using a TiN/TiAlN multilayer coating system Gilberto Bejarano Julio Caicedo Juan Muñoz Saldaña Ingeniería TiN hard coatings TiAlN coatings multilayer system Magnetron sputtering TiN/TiAlN (titanium nitride/titanium aluminum nitride) multilayer were deposited by d.c. reactive magnetron sputtering using titanium and aluminum targets with 10 cm in diameter and 99.9% purity in an argon/nitrogen (Ar/N) atmosphere, applying a substrate temperature of 300°C and a pressure of 7x10-3 mbar. Silicon (100) and heat treated AISI 4340 steel samples with a hardness of 54 Rockwell C (HRC, approximately 5.4 GPa) were utilized as substrate. TiN/TiAlN coatings with 70% aluminum and 4 um total thickness were investigated as function of multilayer number and their mechanical and tribological properties compared to the uncoated steel samples. The crystalline structure of the coated samples was analyzed through X-ray diffractometry and its morphology and topography using scanning electron microscopy (SEM) and atomic force microscopy (AFM). Hardness was determined by means of nanoindentation, while wear resistance was characterized through pin on disc measurements. A hardness and Young Modulus increment from 62% and 70% respectively, were obtained for 150 multilayer of TiN/TiAlN related to 30 bilayers and from 740% and 202% respectively, compared with the uncoated AISI 4340 steel samples. Finally the friction coefficient was reduced from 0.55 down to 0.20 and the roughness from 63 nm to 3.2 nm for the steel samples coated with 150 bilayers of TiN/TiAlN, what conduced to a greater wear resistance of the coating system. 2008 artículo científico 0120-6230 https://www.redalyc.org/articulo.oa?id=43004405 en http://www.redalyc.org/revista.oa?id=430 Revista Facultad de Ingeniería Universidad de Antioquia application/pdf Universidad de Antioquia Revista Facultad de Ingeniería Universidad de Antioquia (Colombia) Num.44
title Mechanical and tribological properties enhancement of heat treated AISI 4340 steel by using a TiN/TiAlN multilayer coating system
topic Ingeniería
TiN
hard coatings
TiAlN coatings
multilayer system
Magnetron sputtering
url https://www.redalyc.org/articulo.oa?id=43004405