Chromatographic analysis of phytochemicals in the peel of Musa paradisiaca to synthesize silver nanoparticles
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| Formato: | Artículo científico |
| Lenguaje: | en |
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Universidad de Antioquia
2022
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| _version_ | 1876484793216008192 |
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| author | María José Buendía-Otero |
| author_facet | María José Buendía-Otero |
| contents | Chromatographic analysis of phytochemicals in the peel of Musa paradisiaca to synthesize silver nanoparticles María José Buendía-Otero Deisy Julieth Jiménez-Corzo Zulia Isabel Caamaño De Ávila Juan B. Restrepo Ingeniería Biosynthesis nanoparticles musa paradisiaca chromatographic analysis This research work used Musa paradisiaca (banana) peels as a natural solvent, assorted with the precursor AgNO3 (10 mM) to perform the green synthesis of silver nanoparticles. The phytochemical components present in the Musa paradisiaca peel extracts were determined by gas chromatography coupled to a mass spectrometer (GC-MS), and it was possible to identify the compounds: 1.2 Ethanediol (60.0261 %) and 2.3 Butanediol (11.2 %); these -diols represent a highly reducing agent for metals, since they act as a solvent for the metal precursor behaving as a reducing agent, and facilitating the formation of nanoparticles. Likewise, the synthesized silver nanoparticles were subjected to a washing and drying treatment to be subsequently characterized by means of UV-Vis and XRD techniques, resulting in a wavelength of 411 nm, which is characteristic of these metallic nanoparticles, and achieving the identification of the face-centered cubic structure (fcc) of the metallic silver, with an average particle size of 21.8 nm according to the Debye-Scherrer equation. 2022 artículo científico 0120-6230 https://www.redalyc.org/articulo.oa?id=43070264012 https://www.redalyc.org/journal/430/43070264012/ https://www.redalyc.org/journal/430/43070264012/html/ https://www.redalyc.org/journal/430/43070264012/43070264012.epub https://www.redalyc.org/journal/430/43070264012/movil 10.17533/udea.redin.20210427 en http://www.redalyc.org/revista.oa?id=430 Revista Facultad de Ingeniería Universidad de Antioquia application/pdf Universidad de Antioquia Revista Facultad de Ingeniería Universidad de Antioquia (Colombia) Num.103 |
| format | Artículo científico |
| id | redalyc_43070264012 |
| institution | Redalyc |
| language | en |
| publishDate | 2022 |
| publisher | Universidad de Antioquia |
| spellingShingle | Chromatographic analysis of phytochemicals in the peel of Musa paradisiaca to synthesize silver nanoparticles María José Buendía-Otero Ingeniería Biosynthesis nanoparticles musa paradisiaca chromatographic analysis Chromatographic analysis of phytochemicals in the peel of Musa paradisiaca to synthesize silver nanoparticles María José Buendía-Otero Deisy Julieth Jiménez-Corzo Zulia Isabel Caamaño De Ávila Juan B. Restrepo Ingeniería Biosynthesis nanoparticles musa paradisiaca chromatographic analysis This research work used Musa paradisiaca (banana) peels as a natural solvent, assorted with the precursor AgNO3 (10 mM) to perform the green synthesis of silver nanoparticles. The phytochemical components present in the Musa paradisiaca peel extracts were determined by gas chromatography coupled to a mass spectrometer (GC-MS), and it was possible to identify the compounds: 1.2 Ethanediol (60.0261 %) and 2.3 Butanediol (11.2 %); these -diols represent a highly reducing agent for metals, since they act as a solvent for the metal precursor behaving as a reducing agent, and facilitating the formation of nanoparticles. Likewise, the synthesized silver nanoparticles were subjected to a washing and drying treatment to be subsequently characterized by means of UV-Vis and XRD techniques, resulting in a wavelength of 411 nm, which is characteristic of these metallic nanoparticles, and achieving the identification of the face-centered cubic structure (fcc) of the metallic silver, with an average particle size of 21.8 nm according to the Debye-Scherrer equation. 2022 artículo científico 0120-6230 https://www.redalyc.org/articulo.oa?id=43070264012 https://www.redalyc.org/journal/430/43070264012/ https://www.redalyc.org/journal/430/43070264012/html/ https://www.redalyc.org/journal/430/43070264012/43070264012.epub https://www.redalyc.org/journal/430/43070264012/movil 10.17533/udea.redin.20210427 en http://www.redalyc.org/revista.oa?id=430 Revista Facultad de Ingeniería Universidad de Antioquia application/pdf Universidad de Antioquia Revista Facultad de Ingeniería Universidad de Antioquia (Colombia) Num.103 |
| title | Chromatographic analysis of phytochemicals in the peel of Musa paradisiaca to synthesize silver nanoparticles |
| topic | Ingeniería Biosynthesis nanoparticles musa paradisiaca chromatographic analysis |
| url | https://www.redalyc.org/articulo.oa?id=43070264012 https://www.redalyc.org/journal/430/43070264012/ https://www.redalyc.org/journal/430/43070264012/html/ https://www.redalyc.org/journal/430/43070264012/43070264012.epub https://www.redalyc.org/journal/430/43070264012/movil |