Nanocrystalline Titanium Oxide thin Films Prepared by Sol-Gel Process

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Auteur principal: Nelcy D. S. Mohallem
Format: Artículo científico
Langue:en
Publié: Sociedade Brasileira de Física 2006
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author Nelcy D. S. Mohallem
author_facet Nelcy D. S. Mohallem
contents Nanocrystalline Titanium Oxide thin Films Prepared by Sol-Gel Process Nelcy D. S. Mohallem Marcelo M. Viana Tarik D. S. Mohallem Gabriel L. T. Nascimento Física, Astronomía y Matemáticas Sol gel process Titanium oxide thin films Crystalline films of pure titanium oxide have been prepared on soda lime slide glasses by sol-gel processand dip-coating. The definition of various parameters such as chemical concentration, viscosity, catalyst typeand withdrawal speed led to the preparation of transparent, crystalline and adherent coatings with hydrophobiccharacteristics. Their crystalline structure was evaluated as anatase phase by low angle X-ray diffraction. Thicknesseswere measured by perfilometry, and the refractive indices were determined from transmittance spectrumtaking into consideration the layers deposited onto the two sides of the substrate. Porosity was also estimatedby UV-visible spectroscopy by using the Lorentz – Lorenz equation. The average grain size was evaluated byatomic force microscopy. The thicker and denser films presented hydrophobicity, which decreased when thefilm porosity increased. 2006 artículo científico 0103-9733 https://www.redalyc.org/articulo.oa?id=46436575 en http://www.redalyc.org/revista.oa?id=464 Brazilian Journal of Physics application/pdf Sociedade Brasileira de Física Brazilian Journal of Physics (Brasil) Num.3B Vol.36
format Artículo científico
id redalyc_46436575
institution Redalyc
language en
publishDate 2006
publisher Sociedade Brasileira de Física
spellingShingle Nanocrystalline Titanium Oxide thin Films Prepared by Sol-Gel Process
Nelcy D. S. Mohallem
Física, Astronomía y Matemáticas
Sol
gel process
Titanium oxide thin films
Nanocrystalline Titanium Oxide thin Films Prepared by Sol-Gel Process Nelcy D. S. Mohallem Marcelo M. Viana Tarik D. S. Mohallem Gabriel L. T. Nascimento Física, Astronomía y Matemáticas Sol gel process Titanium oxide thin films Crystalline films of pure titanium oxide have been prepared on soda lime slide glasses by sol-gel processand dip-coating. The definition of various parameters such as chemical concentration, viscosity, catalyst typeand withdrawal speed led to the preparation of transparent, crystalline and adherent coatings with hydrophobiccharacteristics. Their crystalline structure was evaluated as anatase phase by low angle X-ray diffraction. Thicknesseswere measured by perfilometry, and the refractive indices were determined from transmittance spectrumtaking into consideration the layers deposited onto the two sides of the substrate. Porosity was also estimatedby UV-visible spectroscopy by using the Lorentz – Lorenz equation. The average grain size was evaluated byatomic force microscopy. The thicker and denser films presented hydrophobicity, which decreased when thefilm porosity increased. 2006 artículo científico 0103-9733 https://www.redalyc.org/articulo.oa?id=46436575 en http://www.redalyc.org/revista.oa?id=464 Brazilian Journal of Physics application/pdf Sociedade Brasileira de Física Brazilian Journal of Physics (Brasil) Num.3B Vol.36
title Nanocrystalline Titanium Oxide thin Films Prepared by Sol-Gel Process
topic Física, Astronomía y Matemáticas
Sol
gel process
Titanium oxide thin films
url https://www.redalyc.org/articulo.oa?id=46436575