A Rapid Method for Measurement of Nickel and Chromium at Trace Level in Aqueous Samples

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Autore principale: Muhammad Salman
Natura: Artículo científico
Lingua:en
Pubblicazione: Sociedad Química de México 2011
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author Muhammad Salman
author_facet Muhammad Salman
contents A Rapid Method for Measurement of Nickel and Chromium at Trace Level in Aqueous Samples Muhammad Salman Umer Shafique Waheed -uz-Zaman Rabia Rehman Amna Yousaf Faiza Azhar Jesús M. Anzano Multidisciplinaria (Ciencias Naturales y Exactas) nickel Chromium densitometry image scanning spot test quantification A rapid, simple and portable technique to measure Ni(II) and Cr(VI) at trace level in aqueous samples has been proposed. Colored spots were developed by interacting micro-liter drops of metal solutions with suitable reagents on TLC plates. Soon after, TLC having spots was scanned to import the image into the computer. Color densities of spots were calculated with the help of homemade software. Simple regression was practiced on calibration between standards' concentrations and their color densities. For both metals, correlation coefficients were approaching to one, which pointed out a good correlation between color densities and corresponding analyte concentrations. Real samples from electroplating unit were analyzed with the present and conventional spectrophotometric method (employed as reference), and the results were compared to evaluate the pertinence of the proposed technique in the real analysis. 2011 artículo científico 1870-249X https://www.redalyc.org/articulo.oa?id=47521272004 en http://www.redalyc.org/revista.oa?id=475 Journal of the Mexican Chemical Society application/pdf Sociedad Química de México Journal of the Mexican Chemical Society (México) Num.4 Vol.55
format Artículo científico
id redalyc_47521272004
institution Redalyc
language en
publishDate 2011
publisher Sociedad Química de México
spellingShingle A Rapid Method for Measurement of Nickel and Chromium at Trace Level in Aqueous Samples
Muhammad Salman
Multidisciplinaria (Ciencias Naturales y Exactas)
nickel
Chromium
densitometry
image scanning
spot test quantification
A Rapid Method for Measurement of Nickel and Chromium at Trace Level in Aqueous Samples Muhammad Salman Umer Shafique Waheed -uz-Zaman Rabia Rehman Amna Yousaf Faiza Azhar Jesús M. Anzano Multidisciplinaria (Ciencias Naturales y Exactas) nickel Chromium densitometry image scanning spot test quantification A rapid, simple and portable technique to measure Ni(II) and Cr(VI) at trace level in aqueous samples has been proposed. Colored spots were developed by interacting micro-liter drops of metal solutions with suitable reagents on TLC plates. Soon after, TLC having spots was scanned to import the image into the computer. Color densities of spots were calculated with the help of homemade software. Simple regression was practiced on calibration between standards' concentrations and their color densities. For both metals, correlation coefficients were approaching to one, which pointed out a good correlation between color densities and corresponding analyte concentrations. Real samples from electroplating unit were analyzed with the present and conventional spectrophotometric method (employed as reference), and the results were compared to evaluate the pertinence of the proposed technique in the real analysis. 2011 artículo científico 1870-249X https://www.redalyc.org/articulo.oa?id=47521272004 en http://www.redalyc.org/revista.oa?id=475 Journal of the Mexican Chemical Society application/pdf Sociedad Química de México Journal of the Mexican Chemical Society (México) Num.4 Vol.55
title A Rapid Method for Measurement of Nickel and Chromium at Trace Level in Aqueous Samples
topic Multidisciplinaria (Ciencias Naturales y Exactas)
nickel
Chromium
densitometry
image scanning
spot test quantification
url https://www.redalyc.org/articulo.oa?id=47521272004